Cobalt oxide nanopowder synthesis using cellulose assisted combustion technique

被引:49
作者
Ashok, Anchu [1 ]
Kumar, Anand [2 ]
Bhosale, Rahul R. [2 ]
Saleh, Mohd Ali H. [2 ]
Ghosh, Ujjal Kumar [2 ]
Al-Marri, Mohammed [2 ,3 ]
Almomani, Fares A. [2 ]
Khader, Mahmoud M. [3 ]
Tarlochan, Faris [1 ]
机构
[1] Qatar Univ, Dept Mech & Ind Engn, POB 2713, Doha, Qatar
[2] Qatar Univ, Dept Chem Engn, POB 2713, Doha, Qatar
[3] Qatar Univ, Gas Proc Ctr, POB 2713, Doha, Qatar
关键词
Cellulose assisted combustion synthesis; Solution combustion synthesis; Impregnated layer combustion synthesis; Cobalt oxide nanopowder; LITHIUM-ION BATTERIES; THERMAL-DECOMPOSITION; ETHANOL DECOMPOSITION; HIGHLY EFFICIENT; CO3O4; NANOPARTICLES; PERFORMANCE; CATALYST; NANOMATERIALS; FACILE;
D O I
10.1016/j.ceramint.2016.05.035
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Cobalt oxides nanopowders were prepared using novel cellulose assisted combustion synthesis and solution combustion synthesis techniques. The synthesis conditions were optimized to produce high surface area cobalt oxide nanopowders. Effect of precursors ratio on product properties (such as crystalline structure, nanoparticle size, surface area etc.) were studied and compared for the two methods. Thermodynamic calculations along with TGA/DTA studies were used to understand the synthesis mechanism leading to cobalt oxide formation. The synthesized nanopowders were characterized using various materials characterization techniques such as XRD, SEM and TEM. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:12771 / 12777
页数:7
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