A conical shape-evolution model for the control of sapphire crystal growth in Kyropoulos (KY) method

被引:6
作者
Song, Do Won [1 ,2 ]
Kim, Kwang Seok [3 ]
Kim, Hyo [1 ]
机构
[1] Univ Seoul, Dept Chem Engn, Seoul 130743, South Korea
[2] Siltron Inc, Gumi 730724, Gyeongbuk, South Korea
[3] Korea Gas Safety Corp, Inst Gas Safety R&D, Eumseong Gun 369811, Chungbuk, South Korea
关键词
Conical Shape-evolution Model; Sapphire Crystal; Kyropoulos Method; Mass and Force Balances; Comb-pattern Experiment; DESIGN;
D O I
10.1007/s11814-014-0226-9
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Generally, the process of sapphire crystal growing in the KY furnace has to be monitored in order to reduce the power of heater continuously as the crystal grows to occupy the crucible. However, it has been difficult to control the heater power as the weight and diameter of crystal change because the solid-liquid interface could not be easily located from on-site measurement. Hence, first, the model was developed to locate the crystal-melt interface and to estimate its dynamic feature during the crystal growth by incorporating the mass and the force balances. This model was applied to analyze the data obtained from the industry-scale crystal growth experiment (for the production of the sapphire crystals in the KY method). Finally, the shape and the dynamic feature of crystallizing front are analytically verified by generating some bands of small bubbles along the crystal-melt interface called a comb-pattern experiment.
引用
收藏
页码:486 / 493
页数:8
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