Lu2O3-MgO Nano-powder: Synthesis and Fabrication of Composite Infrared Transparent Ceramics

被引:4
作者
Man Xin [1 ]
Wu Nan [2 ]
Zhang Mu [1 ,3 ]
He Hongliang [4 ]
Sun Xudong [3 ,5 ]
Li Xiaodong [1 ,3 ]
机构
[1] Northeastern Univ, Sch Mat Sci & Engn, Shenyang 110819, Peoples R China
[2] Shenyang Univ, Sch Mech Engn, Shenyang 110044, Peoples R China
[3] Northeastern Univ, Key Lab Anisotropy & Texture Mat, Minist Educ, Shenyang 110819, Peoples R China
[4] China Acad Engn Phys, Inst Fluid Phys, Natl Key Lab Shock Wave & Detonat Phys, Mianyang 621900, Sichuan, Peoples R China
[5] Northeastern Univ, Foshan Grad Sch, Foshan 528311, Peoples R China
基金
中国国家自然科学基金;
关键词
Sol-Gel method; hot-pressing sintering; Lu2O3-MgO; nano-composites; infrared window materials; PHASE HOMOGENEITY; DECOMPOSITION;
D O I
10.15541/jim20210149
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Refining ceramic microstructures to nanometric range to minimize light scattering provides an effective methodology for developing novel optical ceramic materials. In this study, we reported the fabrication and properties of a new nanocomposite optical ceramic of Lu2O3-MgO by using nano powders synthesized via Sol-Gel method and hot-pressing sintering technology. Influence of powder synthesis conditions and hot-pressing sintering process on the microstructure of the sample was investigated, and the theoretical transmittance of the sample was calculated and compared with the measured transmittance. The results show that the Lu2O3-MgO ceramic fabricated by optimizing process exhibts a homogeneous phase domain distribution, a fine-grain size of 123 nm, a high transmittance of 84.5%-86.0% over the 3-5 mu m wavelength range, close to the theoretical transmittance, and enhanced hardness value of 12.2 GPa, toughness value of 2.89 MPa center dot m(-1/2) and bending strength value of (221 +/- 12) MPa, indicating potential application in infrared transparent window material.
引用
收藏
页码:1263 / 1269
页数:7
相关论文
共 22 条
[1]   Transparent alumina: A light-scattering model [J].
Apetz, R ;
van Bruggen, MPB .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2003, 86 (03) :480-486
[2]   Glycine-Nitrate Process for the Elaboration of Eu3+-Doped Gd2O3 Bimodal Nanoparticles for Biomedical Applications [J].
Goglio, Graziella ;
Kaur, Gaganpreet ;
Pinho, Sonia L. C. ;
Penin, Nicolas ;
Blandino, Alexia ;
Geraldes, Carlos F. G. C. ;
Garcia, Alain ;
Delville, Marie-Helene .
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2015, (07) :1243-1253
[3]   Properties of an Infrared-Transparent MgO:Y2O3 Nanocomposite [J].
Harris, Daniel C. ;
Cambrea, Lee R. ;
Johnson, Linda F. ;
Seaver, Robert T. ;
Baronowski, Meghan ;
Gentilman, Richard ;
Scott Nordahl, C. ;
Gattuso, Todd ;
Silberstein, Stephanie ;
Rogan, Patrick ;
Hartnett, Thomas ;
Zelinski, Brian ;
Sunne, Wayne ;
Fest, Eric ;
Poisl, W. Howard ;
Willingham, Charles B. ;
Turri, Giorgio ;
Warren, Cori ;
Bass, Michael ;
Zelmon, David E. ;
Goodrich, Steven M. .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2013, 96 (12) :3828-3835
[4]   Transparent sintered corundum with high hardness and strength [J].
Krell, A ;
Blank, P ;
Ma, HW ;
Hutzler, T ;
van Bruggen, MPB ;
Apetz, R .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2003, 86 (01) :12-18
[5]   Transmission physics and consequences for materials selection, manufacturing, and applications [J].
Krell, Andreas ;
Hutzler, Thomas ;
Klimke, Jens .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2009, 29 (02) :207-221
[6]  
[李江 Li Jiang], 2016, [硅酸盐学报, Journal of the Chinese Ceramic Society], V44, P1302
[7]   Preparation and characteristic of properties of high transmission Nd:YAG transparent ceramic [J].
Liu Wen-Bin ;
Kou Hua-Min ;
Pan Yu-Bai ;
Karaki Tomoaki ;
Li Jiang ;
Guo Jing-Kun .
JOURNAL OF INORGANIC MATERIALS, 2008, 23 (05) :1037-1040
[8]   Fabrication and laser operation of Yb:Lu2O3 transparent ceramics from co-precipitated nano-powders [J].
Liu, Ziyu ;
Toci, Guido ;
Pirri, Angela ;
Patrizi, Barbara ;
Li, Jinbang ;
Hu, Zewang ;
Wei, Jiabei ;
Pan, Hongming ;
Xie, Tengfei ;
Vannini, Matteo ;
Li, Jiang .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2019, 102 (12) :7491-7499
[9]   Influence of microstructure control on optical and mechanical properties of infrared transparent Y2O3-MgO nanocomposite [J].
Ma, Ho Jin ;
Jung, Wook Ki ;
Baek, Changyeon ;
Kim, Do Kyung .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2017, 37 (15) :4902-4911
[10]   Refractive index and optical dispersion of rare earth oxides using a small-prism technique [J].
Medenbach, O ;
Dettmar, D ;
Shannon, RD ;
Fischer, RX ;
Yen, WM .
JOURNAL OF OPTICS A-PURE AND APPLIED OPTICS, 2001, 3 (03) :174-177