Synthesis and crystal structures of non-symmetric 1,3-di(alkyloxy)imidazolium salts

被引：10

作者：

Jochriem, Markus ^{[1
]}

Kirchler, Christian G. ^{[1
]}

Laus, Gerhard ^{[1
]}

Wurst, Klaus ^{[1
]}

Kopacka, Holger ^{[1
]}

Mueller, Thomas ^{[1
]}

Schottenberger, Herwig ^{[1
]}

机构：

[1] Univ Innsbruck, Fac Chem & Pharm, A-6020 Innsbruck, Austria

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 2017年 / 72卷 / 08期

关键词：

imidazolium salt; ionic liquid; mercury; thione; tribromide; IONIC LIQUIDS; DERIVATIVES; TRIBROMIDE; DIBROMINE; HALOGEN;

D O I：

10.1515/znb-2017-0089

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A series of non-symmetric 1,3-di(alkyloxy)imidazolium salts were synthesized by stepwise alkylation of 1-hydroxyimidazole-3-oxide. The quaternary salts were subsequently functionalized by bromination in 2-position. A 2-azidoimidazolium salt and an imidazoline-2-thione were prepared exemplarily. Crystal structures of two 2-bromo-1-alkyloxy-3-methyloxyimidazolium tribromides and a mercury(II)-thione complex have been determined by X-ray diffraction.

引用

页码：617 / 626

页数：10

共 50 条

[41] 1,2-Propanediol-linked chiral symmetric and non-symmetric liquid crystal dimers containing trifluoromethyl
Xu, Zhi-Xin
Yao, Miao
Feng, Wei-Jiao
Liu, Kun-Li
Zhu, Qi
Tian, Mei
Hu, Jian-she
Yao, Dan-Shu
LIQUID CRYSTALS, 2016, 43 (12) : 1846 - 1861
[42] STRUCTURES OF 1,3-DI(9-CARBAZOLYL)PROPANE AND 1,5-DI(9-CARBAZOLYL)PENTANE - POLYVINYLCARBAZOLE MODEL COMPOUNDS
BAKER, RJ
CHEN, ZH
KRAFCIK, RB
MASNOVI, J
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 2167 - 2170
[43] Synthesis and properties of polyimides from 1,3-di(p-dimethylaminobenzyl)-imidazolidine-2-thion
Seckin, T
Çetinkaya, E
Köytepe, S
Yigit, B
POLYMER BULLETIN, 2003, 50 (03) : 139 - 146
[44] Non-Symmetric Liquid Crystal Dimers Containing Azobenzene and 1,3,4-Oxadiazole Group: Synthesis and Mesomorphic Behaviour
Bai, Binglian
Wang, Haitao
Lin, Xiaolong
Ran, Xia
Zhao, Chengxiao
Li, Min
LETTERS IN ORGANIC CHEMISTRY, 2012, 9 (01) : 76 - 80
[45] Non-symmetric liquid crystal dimers containing the 4-nitrobenzohydrazide group: synthesis and mesomorphic behaviour
Bai, Binglian
Wang, Haitao
Zhang, Peng
Qu, Songnan
Li, Fan
Yu, Zhixin
Long, Beihong
Li, Min
LIQUID CRYSTALS, 2008, 35 (07) : 793 - 798
[46] 1,3-Dipolar cycloaddition of azomethine ylides and imidoyl halides for synthesis of π-extended imidazolium salts
Li, Qiang-Qiang
Hamamoto, Yosuke
Tan, Cheryl Cai Hui
Sato, Hiroyasu
Ito, Shingo
ORGANIC CHEMISTRY FRONTIERS, 2022, 9 (15) : 4128 - 4134
[47] Two Metal-Organic Frameworks Constructed by 1,3-Di(1H-imidazol-4-yl) Ligand: Synthesis, Crystal Structure and Photoluminescence Property
Liu, Zhi-Qiang
Wu, Jun-Feng
Chen, Jun
Wu, Xia
Wang, Yan
CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2020, 36 (01) : 159 - 164
[48] Synthesis and properties of new non-symmetric liquid crystal dimers containing mandelic acid and cyano group
Yao, Miao
Chen, Xin-shi
Dong, Liang
Wan, Xin-yi
Xian, Yu-pei
Yao, Dan-shu
Hu, Jian-she
Tian, Mei
LIQUID CRYSTALS, 2018, 45 (06) : 931 - 941
[49] Synthesis and mesomorphic properties of non-symmetric liquid crystal dimers stabilized by benzothiazole and substituted aromatic imines
Al-Taifi, Elham A.
Yeap, Guan-Yeow
Ibrahim, Omaima F.
Marae, Islam S.
Al-Waleedy, Safiyyah A. H.
Bakhite, Etify A.
EGYPTIAN JOURNAL OF CHEMISTRY, 2023, 66 (01): : 419 - 429
[50] Synthesis, Optical and DFT Characterizations of Laterally Fluorinated Phenyl Cinnamate Liquid Crystal Non-Symmetric System
Al-Mutabagani, Laila A.
Alshabanah, Latifah A.
Ahmed, Hoda A.
El-Atawy, Mohamed A.
SYMMETRY-BASEL, 2021, 13 (07):

← 1 2 3 4 5 →