Infrared heat aided solid state synthesis of pyrroles from 1,4-diketones and ammonium acetate

被引：8

作者：

Zhang, Chun ^{[1
]}

Wang, Jian ^{[1
]}

Li, Jing-Hua ^{[1
]}

机构：

[1] Zhejiang Univ Technol, Coll Pharmaceut Sci, Hangzhou 310032, Zhejiang, Peoples R China

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2012年 / 49卷 / 01期

关键词：

H BOND FUNCTIONALIZATION; PROPARGYLIC ALCOHOLS; SEQUENTIAL REACTIONS; SUBSTITUENTS;

D O I：

10.1002/jhet.744

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A facile amination of 1,4-diketones with ammonium acetate has been achieved by mechanochemical grinding assisted by infrared irradiation in the presence of silica gel. The wastes are reduced and the energy resources saved. J. Heterocyclic Chem., (2012).

引用

页码：204 / 207

页数：4

共 51 条

[1]

Albert P. J., 1976, ORG CHEM, V41, P543

[2]

Ballini R, 2000, SYNLETT, P391

[3] Pyrrole syntheses by multicomponent coupling reactions [J].

Balme, G .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2004, 43 (46) :6238-6241

[4] Straightforward highly efficient Paal-Knorr synthesis of pyrroles [J].

Banik, BK ;

Banik, I ;

Renteria, M ;

Dasgupta, SK .

TETRAHEDRON LETTERS, 2005, 46 (15) :2643-2645

[5] Simple synthesis of substituted pyrroles [J].

Banik, BK ;

Samajdar, S ;

Banik, I .

JOURNAL OF ORGANIC CHEMISTRY, 2004, 69 (01) :213-216

[6] Mild aerobic oxidative palladium (II) catalyzed C-H bond functionalization: Regioselective and switchable C-H alkenylation and annulation of pyrroles [J].

Beck, EM ;

Grimster, NP ;

Hatley, R ;

Gaunt, MJ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2006, 128 (08) :2528-2529

[7] Synthesis and biological activity of pyrrole, pyrroline and pyrrolidine derivatives with two aryl groups on adjacent positions [J].

Bellina, Fabio ;

Rossi, Renzo .

TETRAHEDRON, 2006, 62 (31) :7213-7256

[8] Total syntheses of ningalin A, lamellarin O, lukianol A, and permethyl storniamide A utilizing heterocyclic azadiene Diels-Alder reactions [J].

Boger, DL ;

Boyce, CW ;

Labroli, MA ;

Sehon, CA ;

Jin, Q .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1999, 121 (01) :54-62

[9]

Boiko I. I., 2005, P ECSOC 9 INT EL C S, P1

[10] Creative approaches towards the synthesis of 2,5-dihydro- furans, thiophenes, and pyrroles. One method does not at all! [J].

Brichacek, Matthew ;

Njardarson, Jon T. .

ORGANIC & BIOMOLECULAR CHEMISTRY, 2009, 7 (09) :1761-1770

← 1 2 3 4 5 6 →