Synthesis of nanocrystalline Ni2B via a solvo-thermal route

被引：15

作者：

Feng, X

Bai, YJ ^{[1
]}

Lü, B

Zhao, YR

Yang, J

Chi, JR

机构：

[1] Shandong Univ Sci & Technol, Dept Mech Engn, Jinan 250031, Peoples R China

[2] Qingdao Univ, Coll Mech Engn, Qingdao 266071, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2004年 / 7卷 / 02期

关键词：

nickel boride; solvo-thermal route; X-ray powder diffraction; transmission electron microscopy; X-ray photoelectron spectra;

D O I：

10.1016/j.inoche.2003.11.003

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Nickel boride (Ni2B) nanocrystals were successfully synthesized via the reaction of NiCl2 and NaBH4 at 420 degreesC with benzene as solvent. The yield is about 60%. The crystals were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS). Highly crystallized Ni2B with an average size of 20 nm was obtained. (C) 2003 Elsevier B.V. All rights reserved.

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页码：189 / 191

页数：3

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