Facile preparation of graphene oxide films with controllable interlayer distances

被引:6
|
作者
Shen, Jiaxin [1 ]
Hui, Zhiqing [1 ]
Deng, Yunkai [1 ]
Cai, Zhiyuan [1 ]
Huang, Wentao [1 ]
Zhao, Chen [2 ]
Min, Yonggang [1 ]
Epstein, Arthur J. [3 ]
机构
[1] Nanjing Univ Posts & Telecommun, Inst Adv Mat, 9 Wenyuan Rd, Nanjing 210046, Jiangsu, Peoples R China
[2] Guangdong Univ Technol, Sch Mat & Energy, Guangzhou 510006, Guangdong, Peoples R China
[3] Ohio State Univ, Dept Phys & Chem & Biochem, 100 West 18th Ave, Columbus, OH 43210 USA
关键词
Graphene oxide; Interlayer distance; Coagulant; Wet-spinning; SEPARATION MEMBRANES; WATER; PERFORMANCE; TRANSPORT; REMOVAL; FIBERS;
D O I
10.1016/j.jallcom.2017.11.217
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In this work, a facile method to prepare graphene oxide films with controllable interlayer distances similar to that of wet-spinning is proposed. Wet graphene oxide gel films were dipped into coagulation bath for crosslinking. Calcium chloride, two ionic liquids, 1-butyl-3-methylimidazole L lactate and 1-aminopropyl- 3-methylimidazolium chloride and 1,8-octanediamine were chosen as the coagulants. The obtained graphene oxide films were characterized by Fourier transform infrared spectroscopy, Raman spectroscopy, scanning electron microscopy, X-ray diffraction and tensile tests. The adsorption of Rhodamine B solutions tests proved that GO films with different interlayer distances exhibited varied sieving performance. (C) 2017 Elsevier B.V. All rights reserved.
引用
收藏
页码:1514 / 1519
页数:6
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