Correlative electron and X-ray microscopy: probing chemistry and bonding with high spatial resolution

被引：17

作者：

Goode, Angela E. ^{[1
]}

Porter, Alexandra E. ^{[1
]}

Ryan, Mary P. ^{[1
]}

McComb, David W. ^{[2
]}

机构：

[1] Univ London Imperial Coll Sci Technol & Med, Dept Mat, London SW7 2AZ, England

[2] Ohio State Univ, Dept Mat Sci & Engn, Columbus, OH 43210 USA

来源：

NANOSCALE | 2015年 / 7卷 / 05期

基金：

英国工程与自然科学研究理事会;

关键词：

ENERGY-LOSS SPECTROSCOPY; CARBON NANOTUBES; LIQUID CELL; SPECTROMICROSCOPY; ABSORPTION; EELS; NANOPARTICLE; MORPHOLOGY; SPECIATION; OPERANDO;

D O I：

10.1039/c4nr05922k

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Two powerful and complementary techniques for chemical characterisation of nanoscale systems are electron energy-loss spectroscopy in the scanning transmission electron microscope, and X-ray absorption spectroscopy in the scanning transmission X-ray microscope. A correlative approach to spectromicroscopy may not only bridge the gaps in spatial and spectral resolution which exist between the two instruments, but also offer unique opportunities for nanoscale characterisation. This review will discuss the similarities of the two spectroscopy techniques and the state of the art for each microscope. Case studies have been selected to illustrate the benefits and limitations of correlative electron and X-ray microscopy techniques. In situ techniques and radiation damage are also discussed.

引用

页码：1534 / 1548

页数：15

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