Synthesis, characterization and study of mesomorphic behavior of new bent and linear core compounds containing heterocyclic rings

被引:5
作者
Karam, Nisreen H. [1 ]
Shanshal, Alaa K. [1 ]
Al-Dujaili, Ammar H. [2 ]
机构
[1] Univ Baghdad, Coll Educ Pure Sci, Dept Chem, Baghdad, Iraq
[2] Univ Jordan, Hamdi Mango Ctr Sci Res, Amman 11942, Jordan
关键词
1; 3; 4-oxadiazole; heterocyclic; liquid crystal; piperazine; thiazolidin-4-one; LIQUID-CRYSTALS; PYRIMIDINE; PYRAZOLES;
D O I
10.1080/15421406.2021.1966871
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The article presents the synthesis and liquid crystalline properties of some of new bent and linear core compounds containing a 1,3,4-oxadiazole, piperazine and thiazolidin-4-one rings as a central core. The new synthesized compounds were characterized by elemental analysis and FTIR, (HNMR)-H-1 and mass spectroscopy). The liquid crystalline properties were studied by polarized optical microscopy and differential scanning calorimetry. All Schiff bases compounds with 1,3,4-oxadiazole and piprzaine ring in central core presented liquid crystalline properties. The liquid crystallinity of compounds containing 1,3,4-oxadiazole and thiazolidin-4-one rings as a central core were found depending on the type of terminal substituents.
引用
收藏
页码:66 / 79
页数:14
相关论文
共 34 条
[1]   Synthesis, Characterization, and Mesomorphic Properties of New Pyridine Derivatives [J].
Ahipa, T. N. .
CHEMISTRYOPEN, 2015, 4 (06) :786-791
[2]   Synthesis, characterization and liquid crystalline properties of novel benzimidazol-8-hydroxyquinoline complexes [J].
Al-Noor, Taghreed H. ;
Karam, Nisreen H. ;
Ghanim, Faeza H. ;
Kindeel, Alia S. ;
Al-Dujaili, Ammar H. .
INORGANICA CHIMICA ACTA, 2017, 466 :612-617
[3]   4-Methylresorcinol based bent-core liquid crystals with azobenzene wings - a new class of compounds with dark conglomerate phases [J].
Alaasar, Mohamed ;
Prehm, Marko ;
Brautzsch, Marcel ;
Tschierske, Carsten .
JOURNAL OF MATERIALS CHEMISTRY C, 2014, 2 (28) :5487-5501
[4]  
Baia A.M, 2009, REV CHIM-BUCHAREST, V60, P1021
[5]   Stimuli-Driven Control of the Helical Axis of Self-Organized Soft Helical Superstructures [J].
Bisoyi, Hari Krishna ;
Bunning, Timothy J. ;
Li, Quan .
ADVANCED MATERIALS, 2018, 30 (25)
[6]   Symmetric Bent-core Liquid Crystals of Some Schiff Bases Containing Azo Linkage [J].
Ciobanu, Catalina Ionica ;
Carlescu, Irina ;
Lisa, Gabriela ;
Scutaru, Dan .
CROATICA CHEMICA ACTA, 2014, 87 (01) :7-16
[7]   New 1,4-diaryl [1,2,3]-triazole liquid crystals using a click reaction [J].
Conte, G ;
Cristiano, R ;
Ely, F ;
Gallardo, H .
SYNTHETIC COMMUNICATIONS, 2006, 36 (07) :951-958
[8]  
Gray G.W., 1984, SMECTIC LIQUID CRYST
[9]   Conductive liquid crystalline compounds having a piperazine structure [J].
Haramoto, Y ;
Yamada, T ;
Nanasawa, M ;
Funahashi, M ;
Hanna, J ;
Ujiie, S .
LIQUID CRYSTALS, 2002, 29 (08) :1109-1111
[10]   New cholesteryl-containing bent core liquid crystals [J].
Huzum, Cosmin-Constantin ;
Carlescu, Irina ;
Lisa, Gabriela ;
Scutaru, Dan .
JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 2013, 78 (05) :669-680