Synthesis and Characterization of Novel Polyamines Containing Different Substitute Groups Via Chemical Oxidative Polymerization

被引：4

作者：

Senol, Dilek ^{[1
]}

Kaya, Ismet ^{[1
]}

机构：

[1] Canakkale Onsekiz Mart Univ, Fac Sci & Arts, Dept Chem, Polymer Synth & Anal Lab, TR-17020 Canakkale, Turkey

来源：

JOURNAL OF THE CHINESE CHEMICAL SOCIETY | 2015年 / 62卷 / 05期

关键词：

Oxidative polycondensation; Substituted aromatic amines; Thermal analysis; Electrical conductivity; Band gap; ELECTROCHEMICAL PROPERTIES; ELECTRICAL-CONDUCTIVITY; THERMAL-STABILITY; SOLUBILITY; POLYMERS;

D O I：

10.1002/jccs.201400525

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In this study, polymers of substitute aromatic amine compounds were synthesized by chemical oxidative polycondensation in aqueous alkaline medium using NaOCl as oxidant. The structures of synthesized compounds were confirmed by FT-IR, UV-Vis and NMR analyses. The characterizations of synthesized compounds were made by fluorescence, TG-DTA, DSC, scanning electron microscopy (SEM) and Brunauer-Emmett-Teller (BET) surface area measurements. In addition, electrochemical and electrical conductivity values of compounds were carried out with cyclic voltammetry (CV) and four points probe technique measurements, respectively. Synthesized polymers viewed structural change, optical, electrochemical and thermal differences.

引用

页码：429 / 438

页数：10

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