Comparison of two analytical methods (ELISA and LC-MS/MS) for determination of aflatoxin B1 in corn and aflatoxin M1 in milk

被引：25

作者：

Stefanovic, Srdjan ^{[1
]}

Spiric, Danka ^{[1
]}

Petronijevic, Radivoj ^{[1
]}

Trailovic, Jelena Nedeljkovic ^{[2
]}

Milicevic, Dragan ^{[1
]}

Nikolic, Dragica ^{[1
]}

Jankovic, Sasa ^{[1
]}

机构：

[1] Inst Meat Hyg & Technol, Kacanskog 13, Belgrade 11000, Serbia

[2] Univ Belgrade, Fac Vet Med, Belgrade 11000, Serbia

来源：

58TH INTERNATIONAL MEAT INDUSTRY CONFERENCE (MEATCON2015) | 2015年 / 5卷

关键词：

aflatoxin B1; aflatoxin M1; corn; milk; ELISA; LC-MS/MS; MYCOTOXINS;

D O I：

10.1016/j.profoo.2015.09.077

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

The aim of this paper is to assess the closeness of agreement between results of ELISA and LC-MS/MS methods for determination of aflatoxin B-1 in corn and aflatoxin M-1 in milk. Samples of corn (n=100) and milk (n=250) were simultaneously analyzed using ELISA and LC-MS/MS methods, after the severe drought that affected Serbia in summer 2012 resulting in occurrence of aflatoxin B1 in corn and aflatoxin M-1 in milk. Regression analysis showed higher level of agreement between aflatoxin B-1 samples (R2=0.994), compared to aflatoxin M-1 samples (r(2)=0.920). However, both techniques were satisfactory in meeting the requirements for official control purposes. (C) 2015 The Authors. Published by Elsevier Ltd.

引用

页码：270 / 273

页数：4

共 8 条

[1] Update of survey, regulation and toxic effects of mycotoxins in Europe
Creppy, EE
[J]. TOXICOLOGY LETTERS, 2002, 127 (1-3) : 19 - 28
[2] *FAO, 1996, BAS FACTS WORLD CER
[3] IARC, 2002, IARC MONOGRAPHS EVAL, P1
[4] Milicevic D., 2014, Tehnologija Mesa, V55, P22, DOI 10.5937/tehmesa1401022M
[5] RHMZ, 2013, RHMZ SEZ BILT 2012
[6] Determination of mycotoxins in bovine milk by liquid chromatography tandem mass spectrometry
Sorensen, LK
Elbæk, TH
[J]. JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2005, 820 (02): : 183 - 196
[7] New strategies for the screening and determination of aflatoxins and the detection of aflatoxin-producing moulds in food and feed
Stroka, J
Anklam, E
[J]. TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2002, 21 (02) : 90 - 95
[8] Development and validation of a liquid chromatography/tandem mass spectrometric method for the determination of 39 mycotoxins in wheat and maize
Sulyok, Michael
Berthiller, Franz
Krska, Rudolf
Schuhmacher, Rainer
[J]. RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2006, 20 (18) : 2649 - 2659

← 1 →