Crystal structure of N-((3R,10S,13S,17S)-17-((S)-1-(dimethylamino)ethyl)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)-N-methylbenzamide, C31H48N2O

被引：4

作者：

Tan, Bo ^{[2
,3
]}

Wu, Qi-Yun ^{[2
,3
]}

Wu, Ji-Chun ^{[2
]}

Huo, Shao-Jie ^{[2
]}

He, Xi-Cheng ^{[2
]}

Du, Jiang ^{[1
]}

机构：

[1] Guiyang Coll Tradit Chinese Med, Coll Pharm, Guiyang 550025, Guizhou, Peoples R China

[2] Guiyang Coll Tradit Chinese Med, Guiyang 550025, Guizhou, Peoples R China

[3] Key Lab Miao Med Guizhou Prov, Guiyang 550025, Guizhou, Peoples R China

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2019年 / 234卷 / 03期

基金：

中国国家自然科学基金;

关键词：

STEROIDAL ALKALOIDS; SARCOCOCCA-HOOKERIANA;

D O I：

10.1515/ncrs-2018-0557

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

C31H48N2O, orthorhombic, P2(1)2(1)2(1) (no. 19), a = 6.530(2) angstrom, b = 11.728(4) angstrom, c = 35.236(12) angstrom, V = 2698.6(15) angstrom(3), Z = 4, R-gt(F) = 0.0492, wR(ref)(F-2) = 0.1034, T = 173 K.

引用

页码：551 / 553

页数：3

共 5 条

[1] Crystal structure of (E)-N-((3R,5S,10S, 13S,14S,17S)-17-((S)-1-(dim ethylamino)ethyl)-10,13-dimethylhexadecahydro-1H-cyclopenta[a] phenanthren-3-yl)-2-methylbut-2-enamide - water - methanol (1/1/1), C29H54N2O3
Tan, Bo
Wu, Qi-Yun
Wu, Ji-Chun
Huo, Shao-Jie
He, Xi-Cheng
Du, Jiang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (04): : 801 - 803
[2] Crystal structure of (E)-N-((2S,3S,4R,10R,13S,17S)-17-(1-(dimethylamino)ethyl)-2,4-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)-2-methylbut-2-enamide, C24H48N2O3
Wu, Qi-Yun
Wu, Ji-Chun
Huo, Shao-Jie
He, Xi-Chen
Du, Jiang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (03): : 513 - 516
[3] Synthesis and crystal structure of-(3S,10S,13S,17S)-N-(2-methoxyphenyl)-10,13-dimethyl-17-((R)-1-(p-tolylamino)ethyl)hexadecahydro-1H-cyclopenta[α]phenanthren-3-amine, C35H50N2O
Yang, Mei
Wei, Peng
Sun, Yi-Chun
Ye, Jiang-Hai
Zou, Juan
He, Kang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2025, 240 (02): : 221 - 223
[4] Synthesis and crystal structure of 1-((3R,10S,13R,17S)-10,13-dimethyl-3-(phenylamino)hexadecahydro-1H-cyclopenta[α] phenanthren-17-yl)ethan-1-one, C27H39NO
Zhang, Wen-Wen
Ye, Jiang-Hai
Zou, Juan
He, Kang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2022, 237 (05): : 815 - 817
[5] Crystal structure of (1S)-N-(chloromethyl)-1-((4S,6aR,8aS, 8bR, 9aR)-4-methoxy-6a,8a-dimethyl-1,3,4, 5,6,6a,6b,7,8,8a,9a,10,10a, 10b-tetradecahydro-8bH-naphtho[2′,1′:4,5] indeno[1,2-b]oxiren-8b-yl)-N-methylethan-1-amine, C24H46ClNO5
Ning, Xue-Jing
Yang, Xiao-Bin
Du, Jiang
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2020, 235 (06): : 1493 - 1494

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