Stabilization heat treatment and functional response of 0.65[Pb(Mg1/3Nb2/3)O3]-0.35[PbTiO3] ceramics

被引：7

作者：

Augustine, Pius ^{[1
,2
,3
,4
]}

Samanta, Shibnath ^{[5
]}

Rath, Martando ^{[1
,2
]}

Miryala, Muralidhar ^{[4
]}

Sethupathi, K. ^{[5
]}

Murakami, Masato ^{[4
]}

Rao, M. S. Ramachandra ^{[1
,2
]}

机构：

[1] Indian Inst Technol, Nano Funct Mat Technol Ctr, Dept Phys, Madras 600036, Tamil Nadu, India

[2] Indian Inst Technol, Mat Sci Res Ctr, Madras 600036, Tamil Nadu, India

[3] Sacred Heart Coll Autonomous, Dept Phys, Kochi 682013, Kerala, India

[4] Shibaura Inst Technol, Grad Sch Sci & Engn, Superconducting Mat Lab, Koto Ku, 3-7-5 Toyosu, Tokyo 1358548, Japan

[5] Indian Inst Technol, Low Temp Phys Lab, Dept Phys, Madras 600036, Tamil Nadu, India

来源：

MATERIALS RESEARCH BULLETIN | 2017年 / 95卷

关键词：

Ceramics; Microstructure; Piezoelectricity; Ferroelectricity; Dielectric properties; MORPHOTROPIC PHASE-BOUNDARY; FERROELECTRIC CERAMICS; DIELECTRIC-PROPERTIES; SINGLE-CRYSTALS; ELECTRICAL-PROPERTIES; THICK-FILMS; PMN-PT; RELAXOR; TEMPERATURE; SYSTEM;

D O I：

10.1016/j.materresbull.2017.07.019

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

We report on the heat treatment to stabilize 0.65[Pb(Mg1/3Nb2/3)O-3]-0.35[PbTiO3] ceramics and its effect on the functional response. The stabilization heat treatment at 1050 degrees C for 4 h was effective in removing un-reacted PbO from the ceramics, which was confirmed through the measurements of dielectric and ferroelectric properties for a series of samples with different PbO contents. We also found that the stage of the stabilization heat treatment affected the sample properties. When this treatment was administrated to the sample during calcination, it exhibited excellent ferroelectric behavior. On the other hand, the same stabilization heat treatment given to the compacted pellet prior to sintering resulted in excellent dielectric properties with comparatively low ferroelectric hysteresis. (C) 2017 Elsevier Ltd. All rights reserved.

引用

页码：47 / 55

页数：9

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