Reaction chemistry during self-propagating high-temperature synthesis (SHS) of H3BO3-ZrO2-Mg system

被引：15
|
作者：
Khanra, A. K. [1 ]
机构：
[1] Indian Inst Technol, Dept Met & Mat Engn, Kharagpur 721302, W Bengal, India
来源：
MATERIALS RESEARCH BULLETIN | 2007年 / 42卷 / 12期
关键词：
carbides; ceramics; electron microscopy; X-ray diffraction; defects;
D O I：
10.1016/j.materresbull.2007.01.016
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
In the present investigation, the ZrB2 powder is produced by SHS of mixture containing H3BO3, ZrO2 and Mg. The thermal analysis and XRD study reveal the reaction mechanism of ZrB2 formation by SHS process. Synthesis of H3BO3-Mg System results in formation Of Mg-3(BO3)(2) and MgB4 phases, whereas ZrO2 is partially reduced to ZrO3 and Zr during synthesis of ZrO2-Mg system. The reaction between elemental Zr and MgB4 results in ZrB2 formation. The particle size of ZrB2 is found to decrease with the addition of SHS diluent. (c) 2007 Elsevier Ltd. All rights reserved.
引用
收藏
页码：2224 / 2229
页数：6
相关论文
共 50 条
  • [21] Dissolution-precipitation-decomposition-crystallization mechanism of self-propagating high-temperature synthesis of Al3Ni2
    Li, Yi
    Nan, Ya-xiong
    Guo, Wei-xiang
    Che, Han-qing
    Fan, Qun-cheng
    INTERMETALLICS, 2010, 18 (01) : 179 - 187
  • [22] Formation mechanism of TiC-Al2O3-Fe3Al composites during self-propagating high-temperature synthesis of TiO2-Al-C-Fe system
    Sharifitabar, M.
    Khaki, J. Vandati
    Sabzevar, M. Haddad
    CERAMICS INTERNATIONAL, 2016, 42 (10) : 12361 - 12370
  • [23] Effect of NaCl on the synthesis of TiB2 powder by a self-propagating high-temperature synthesis technique
    Khanra, AK
    Pathak, LC
    Mishra, SK
    Godkhindi, MM
    MATERIALS LETTERS, 2004, 58 (05) : 733 - 738
  • [24] Investigation of the reaction between Fe2O3 and Al accomplished by Ball Milling and Self-Propagating High-Temperature techniques
    Cao, G
    Concas, G
    Corrias, A
    Orru, R
    Paschina, G
    Simoncini, B
    Spano, G
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION A-A JOURNAL OF PHYSICAL SCIENCES, 1997, 52 (6-7): : 539 - 549
  • [25] Self-propagating high temperature synthesis (SHS) of ZrC-TiC nanocomposites: Comparison of Mg and Al reductant usage and process optimization
    Bugdayci, Mehmet
    Baslayici, Serkan
    Coban, Ozan
    Kaya, Faruk
    JOURNAL OF THE AUSTRALIAN CERAMIC SOCIETY, 2024, 60 (05) : 1541 - 1555
  • [26] High-temperature compressive properties of TiC-TiB2/Cu composites prepared by self-propagating high-temperature synthesis
    Liu, Li-Zhu
    Ying, Guo-Bing
    Zhu, Jia
    Lin, Hong
    Zhu, Chun-Cheng
    RARE METALS, 2014, 33 (01) : 95 - 98
  • [27] Characteristics of Al2O3-SiC composite powder prepared by the self-propagating high-temperature synthesis process and its sintering behavior
    Lee, JH
    An, CY
    Won, CW
    Cho, SS
    Chun, BS
    MATERIALS RESEARCH BULLETIN, 2000, 35 (06) : 945 - 954
  • [28] Effect of Ni content on the products of Ni-Ti-B system via self-propagating high-temperature synthesis reaction
    Huang, L.
    Wang, H. Y.
    Li, Q.
    Yin, S. Q.
    Jiang, Q. C.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2008, 457 (1-2) : 286 - 291
  • [29] Laser-induced self-propagating synthesis of Al3BC3 powder for high-temperature electromagnetic wave absorption
    Lv, Junyi
    Li, Tao
    Li, Yage
    Li, Hang
    Xia, Zhiwen
    Zhang, Shaowei
    Zhang, Haijun
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2025, 108 (04)
  • [30] Mechanical Activation Assisted Self-Propagating High-Temperature Synthesis of HfB2-HfC Composites
    Zaitsev, A. A.
    Potanin, A. Yu.
    Pogozhev, Yu. S.
    Filonenko, I. O.
    Levashov, E. A.
    INTERNATIONAL JOURNAL OF SELF-PROPAGATING HIGH-TEMPERATURE SYNTHESIS, 2023, 32 (02) : 157 - 168
12345