1-(2,4-dinitrophenyl)-3-(2-hydroxy-5-methylphenyl)-pyrazole-4-carboxaldehyde

被引:3
作者
Jeyakanthan, J
Velmurugan, D
Selvi, S
Perumal, PT
机构
[1] Univ Madras, Dept Crystallog & Biophys, Chennai 600025, India
[2] Cent Leather Res Inst, Organ Div, Chennai 600020, India
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2001年 / 57卷
关键词
D O I
10.1107/S1600536801006900
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C17H12N4O6, the dinitrophenyl and 2-hydroxy-5-methylphenyl groups are oriented with dihedral angles of 23.9 (1) and 13.1 (1)degrees, respectively, with respect to the pyrazole ring. The internal C-C-C ring angles at the ortho and para positions where NO2 is bonded are 121.7 (2) and 121.9 (2)degrees. The dihedral angle between the phenyl rings is 11.2 (1)degrees. The crystal structure is stabilized by O-H . . .N intramolecular and by C-H . . .O intermolecular hydrogen bonds.
引用
收藏
页码:O474 / O476
页数:3
相关论文
共 50 条
  • [21] (E)-1-(2,4-Dinitrophenyl)-2-pentylidenehydrazine
    Neunfeldt, Patricia D.
    Duval, Auri R.
    Cunico, Wilson
    Wardell, Solange M. S. V.
    Tiekink, Edward R. T.
    Wardell, James L.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O483 - U3565
  • [22] ATTEMPTED SYNTHESIS OF 1-(2,4-DINITROPHENYL)-3-METHYL-5-PYRAZOLONE
    CLARKE, PA
    LIMON, CR
    CHEMISTRY & INDUSTRY, 1965, (36) : 1562 - &
  • [23] 3-{1-[(2,4-Dinitrophenyl)hydrazino]ethylidene}-5-(1-methylpropyl)pyrrolidine-2,4-dione
    Siegel, David
    Merkel, Stefan
    Koch, Matthias
    Emmerling, Franziska
    Nehls, Irene
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O988 - U1739
  • [24] N′-[(1E)-1-(2-Hydroxy-5-methylphenyl)ethylidene]-4-methoxybenzohydrazide
    Chang, Jian-Guo
    Ji, Chang-You
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3212 - U3494
  • [25] N′-[1-(2-hydroxy-5-methylphenyl)ethyl-idene]benzenesulfonohydrazide
    Laila, Musalem
    Ali, Hapipah M.
    Puvaneswary, Subramaniam
    Robinson, Ward T.
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1769 - U2062
  • [26] Ethyl 3-methyl-1-(2,4-dinitrophenyl)-1H-pyrazole-4-carboxylate
    Etti, S
    Shanmugam, G
    Ponnuswamy, MN
    Sridhar, R
    Murugan, R
    Perumal, PT
    Ravikumar, K
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2003, 59 : O1835 - O1837
  • [27] (E)-1-(2,4-Dinitrophenyl)-2-(3-ethoxy-4-hydroxybenzylidene)hydrazine
    Fun, Hoong-Kun
    Chantrapromma, Suchada
    Ruanwas, Pumsak
    Kobkeatthawin, Thawanrat
    Kumar, C. S. Chidan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O89 - +
  • [28] 1-(2,4-Dinitrophenyl)-2-[(E)-(3,4,5-trimethoxybenzylidene)]hydrazine
    Chantrapromma, Suchada
    Ruanwas, Pumsak
    Boonnak, Nawong
    Kumar, C. S. Chidan
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0188 - +
  • [29] 2-Hydroxy-N′-[(1Z)-1-(2-hydroxy-5-methylphenyl)-2-methylpropylidene]benzohydrazide
    Chang, Jian-Guo
    Zhao, Ren-Gao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O197 - U4287
  • [30] (4-Chlorophenyl)(2-hydroxy-5-methylphenyl)methanone
    Naveen, S.
    Venu, T. D.
    Shashikanth, S.
    Sridhar, M. A.
    Prasad, J. Shashidhara
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2233 - O2234