N′-(2-Bromo-5-hydroxy-4-methoxybenzylidene)-3,5-dihydroxybenzohydrazide methanol monosolvate

被引:4
作者
Wang, Zong-Gui [2 ]
Yuan, Ling [3 ]
Zhou, Li [4 ]
Nan, Yi [1 ]
机构
[1] Ningxia Med Univ, Tradit Chinese Med Coll, Yinchuan 750004, Ningxia Prov, Peoples R China
[2] Jilin Univ, Hosp 2, Changchun 130041, Jilin Province, Peoples R China
[3] Ningxia Med Univ, Coll Pharm, Yinchuan 750004, Ningxia Prov, Peoples R China
[4] Minzu Univ China, Minor Tradit Med Ctr, Beijing 100081, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词
D O I
10.1107/S1600536811008695
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the crystal structure of the title compound, C15H13BrN2O5 center dot CH3OH, the methanol solvent molecule links symmetry-related molecules through O-H...O and N-H...O hydrogen bonds. Further intermolecular O-H...O hydrogen bonds link symmetry-related molecules, leading to the formation of a three-dimensional network. Two of the H atoms involved in hydrogen bonding are disordered. The dihedral angle between the rings is 5.64 (14)degrees.
引用
收藏
页码:O841 / U187
页数:10
相关论文
共 11 条
[1]   2-Pyrrolythiones as monoanionic bidentate N,S-chelators:: Synthesis and molecular structure of 2-pyrrolylthionato complexes of nickel(II), cobalt(III), and mercury(II) [J].
Brückner, C ;
Rettig, SJ ;
Dolphin, D .
INORGANIC CHEMISTRY, 2000, 39 (26) :6100-6106
[2]  
Bruker, 2001, SMART
[3]  
Bruker, 2003, SAINT PLUS
[4]   catena-Poly[[{2,4-dichloro-6-[2-(ethylamino)ethyliminomethyl]phenolato}copper(II)]-μ-azido] [J].
Diao, Yun-Peng ;
Shu, Xiao-Hong ;
Zhang, Bao-Jing ;
Zhen, Yu-Hong ;
Kang, Ting-Guo .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :M1816-U438
[5]   catena-Poly[[(N,N-dimethylethane-1,2-diamine)-copper(II)]-di-μ1,1-azido-[(N,N-dimethylethane-1,2-diamine)copper(II)]-di-μ1,3-azido] [J].
Diao, Yun-Peng .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :M1081-M1083
[6]   Dioxygen activation by a dinuclear nickel thiolate complex: structural characterization of the ligand oxidized product [J].
Harrop, TC ;
Olmstead, MM ;
Mascharak, PK .
CHEMICAL COMMUNICATIONS, 2003, (03) :410-411
[7]   6-chloro-N′-(3,5-dibromo-2-hydroxybenzylidene)nicotinohydrazide [J].
Huang, Shan-Shan ;
Zhou, Qin ;
Diao, Yun-Peng .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :O4659-U4591
[8]   Azido{2,4-dibromo-6-[2-(diethylamino)ethyliminomethyl]phenolato} copper(II) [J].
Li, Kun ;
Zhang, Hong ;
Wang, Xiao-Na ;
Peng, Jin-Yong ;
Diao, Yun-Peng .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :M2271-U234
[9]   Synthesis, biological evaluation, and quantitative structure-activity relationship analysis of new Schiff bases of hydroxysemicarbazide as potential antitumor agents [J].
Ren, SJ ;
Wang, R ;
Komatsu, K ;
Bonaz-Krause, P ;
Zyrianov, Y ;
McKenna, CE ;
Csipke, C ;
Tokes, ZA ;
Lien, EJ .
JOURNAL OF MEDICINAL CHEMISTRY, 2002, 45 (02) :410-419
[10]  
Sheldrick G.M., 2003, SADABS