2,4,6-trichloro-1,3,5-triazine-promoted synthesis of 1,8-dioxo-octahydroxanthenes under solvent-free conditions

被引:82
作者
Zhang, Zhan-Hui [1 ]
Tao, Xu-Ye [1 ]
机构
[1] Hebei Normal Univ, Coll Chem & Mat Sci, Shijiazhuang, Peoples R China
关键词
D O I
10.1071/CH07274
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A practical protocol has been developed for the synthesis of 1,8-dioxo-octahydroxanthenes from aromatic aldehydes and 5,5-dimethylcyclohexane-1,3-dione under solvent-free conditions in the presence of wet 2,4,6-trichloro-1,3,5-triazine ( TCT, cyanuric chloride). The desired products were obtained in high yields with a simple and environmentally benign procedure.
引用
收藏
页码:77 / 79
页数:3
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