Fabrication and characterization of porous mullite coating on porous silicon carbide support

被引:3
作者
Wang, N [1 ]
Yang, XZ [1 ]
Li, JB [1 ]
Lin, H [1 ]
Chi, B [1 ]
机构
[1] Tsinghua Univ, Dept Mat Sci & Engn, State Key Lab New Ceram & Fine Proc, Beijing 100084, Peoples R China
来源
HIGH-PERFORMANCE CERAMICS III, PTS 1 AND 2 | 2005年 / 280-283卷
关键词
porous; mullite coating; sol-gel; dip-coating; OXIDATION BEHAVIOR; TEMPERATURE;
D O I
10.4028/www.scientific.net/KEM.280-283.1301
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Mullite powders of stoichiometric composition were synthesized by sol-gel process with TEOS and Al(NO3)(3).9H(2)O as silicon and aluminum source. Homogeneous mullite powders were used as the starting materials to prepare the porous mullite coating on the porous silicon carbide support by repeated dip-coating method. XRD analysis revealed that the mullite precursor gels almost completely transformed to orthorhombic crystalline mullite at 1200degreesC. The average pore diameter and porosity of the porous mullite coating were about 4.5mum and 52.3%, respectively.
引用
收藏
页码:1301 / 1304
页数:4
相关论文
共 9 条
[1]   Low temperature pressureless sintering of sol-gel derived mullite [J].
Amutharani, D ;
Gnanam, FD .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1999, 264 (1-2) :254-261
[2]  
KOU DH, 1998, J EUR CERAM SOC, V18, P54
[3]  
Lee KN, 1996, J AM CERAM SOC, V79, P620, DOI 10.1111/j.1151-2916.1996.tb07920.x
[4]   MULLITE FORMATION FROM NONSTOICHIOMETRIC DIPHASIC PRECURSORS [J].
LI, DX ;
THOMSON, WJ .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1991, 74 (10) :2382-2387
[5]  
Li SB, 2003, MATER CHEM PHYS, V78, P655, DOI 10.1016/S0254-0584(02)00301-2
[6]  
RAGER H, 1990, AM MINERAL, V75, P392
[7]   Characterization of macroscopic structural disorder in porous media using mercury porosimetry [J].
Rigby, SP ;
Fletcher, RS ;
Riley, SN .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2001, 240 (01) :190-210
[8]  
TOULOUHAIN YS, 1977, TERMOPHYSICAL PROPER
[9]   Monolithic diphasic gels of mullite by sol-gel process under ultrasound stimulation [J].
Vollet, DR ;
Donatti, DA ;
Domingos, RN ;
de Oliveira, I .
ULTRASONICS SONOCHEMISTRY, 1998, 5 (02) :79-81