Exploiting green sorbents in rotating-disk sorptive extraction for the determination of parabens by high-performance liquid chromatography with tandem electrospray ionization triple quadrupole mass spectrometry

被引:25
作者
Vieira, Camila M. S. [1 ]
Mazurkieviczi, Melaine [1 ]
Lopez Calvo, Angela Maria [2 ]
Debatin, Vitor [1 ]
Micke, Gustavo Amadeu [1 ]
Richter, Pablo [3 ]
Rosero-Moreano, Milton [2 ]
da Rocha, Eduardo Carasek [1 ]
机构
[1] Univ Fed Santa Catarina, Dept Quim, BR-88040900 Florianopolis, SC, Brazil
[2] Univ Caldas, Fac Ciencias Exactas & Nat, Dept Quim, GICTA, Manizales, Colombia
[3] Univ Chile, Dept Quim Inorgan & Analitica, Fac Ciencias Quim & Farmaceut, Santiago, Chile
关键词
cork; montmorillonite clay; parabens; rotating; disk sorptive extraction; water; MOLECULARLY IMPRINTED POLYMER; SOLID-PHASE MICROEXTRACTION; POLYCYCLIC AROMATIC-HYDROCARBONS; PUBLIC-HEALTH SIGNIFICANCE; HUMAN BREAST-TUMORS; WATER SAMPLES; WASTE-WATER; HPLC DETERMINATION; HUMAN URINE; CORK;
D O I
10.1002/jssc.201800426
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
In this study, the viability of applying cork and montmorillonite clay modified with ionic liquid as biosorbents in the rotating-disk sorptive extraction technique was investigated. Specifically, this was aimed at the determination of methyl paraben, ethyl paraben, propyl paraben, and isobutyl paraben, with separation/determination by high-performance liquid chromatography coupled with mass spectrometry. The optimization of the method for both biosorbents was performed using multivariate procedures. The extraction efficiencies for the target compounds in aqueous matrices were compared to those obtained using the commercial sorbent Octadecil Silano-C18. The optimum extraction conditions for both natural sorbents were the use of an ammonia solution (pH 10) as desorption solvent and an extraction time of 30 min. The proposed methods show limits of quantification of 0.8 mu g/L for cork, 3.0 mu g/L for montmorillonite clay and 6.0 mu g/L for Octadecil Silano-C18. The relative recoveries from river water and tap water samples ranged from 80.3 to 118.7% and 80.0 to 119.9% for cork and montmorillonite clay modified with ionic liquid, respectively. Relative standard deviations were obtained for intra-and interday precisions of <15% and <19% for cork and <19% and <17% for montmorillonite clay modified with ionic liquid.
引用
收藏
页码:4047 / 4054
页数:8
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