Synthesis and characterization of manganese ferrite nanoparticles obtained by electrochemical/chemical method

被引：37
|
作者：
Mazario, E. [1 ]
Mayoral, A. [2 ]
Salas, E. [3 ]
Menendez, N. [1 ]
Herrasti, P. [1 ]
Sanchez-Marcos, J. [1 ]
机构：
[1] Univ Autonoma Madrid, Fac Ciencias, Dept Quim Fis Aplicada, C Francisco Tomas y Valiente 7, E-28049 Madrid, Spain
[2] Univ Zaragoza, Inst Nanociencia Aragon, LMA, Mariano Esquillor S-N, Zaragoza 50018, Spain
[3] Spline Spanish CRG Beamline European Synchrotron, ESRF, F-38043 Grenoble, France
来源：
MATERIALS & DESIGN | 2016年 / 111卷
关键词：
Electrochemical synthesis; Superparamagnetic; Nanoparticles; Manganese ferrite; CATION DISTRIBUTION; MAGNETIC-PROPERTIES; NANOCRYSTALS; NEUTRON;
D O I：
10.1016/j.matdes.2016.09.031
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A combined electrochemical/chemicalmethodwas developed in order to synthesize manganese ferrite nanoparticles. The synthesis was carried out in an electrochemical cell containing iron as anode and cathode electrodes and an electrolyte solution of manganese chloride and tetrabutyl ammonium bromide. A usual XRD, STEM compositional mapping images and ICP analysis showed the formation of spinel structure and the presence of Mn, Fe and O in the nanoparticles (NPs) with a stoichiometry Mn0.5Fe2.5O4. The nanoparticle size, shape, and morphology were characterized using electron microscopy and X-Ray absorption spectroscopy, and SQUID measurements were carried out to determine the magnetic behavior. This sample was compared with a same composition manganese ferrite obtained by electrochemical synthesis. (C) 2016 Elsevier Ltd. All rights reserved.
引用
收藏
页码：646 / 650
页数：5
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