1,5-Dimethyl-2-phenyl-4-{[(E)-3,4,5-trimethoxybenzylidene]amino}-1H-pyrazol-3(2H)-one

被引：0
|
作者：
Liu, Shan-Bin [1 ]
Bi, Cai-Feng [1 ]
Fan, Yu-Hua [1 ]
Zhang, Xia [1 ]
Zhang, Dong-Mei [1 ]
机构：
[1] Ocean Univ China, Coll Chem & Chem Engn, Minist Educ, Key Lab Marine Chem Theory & Technol, Qingdao 266100, Shandong, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
基金：
美国国家科学基金会;
关键词：
SCHIFF-BASE LIGANDS; COMPLEXES;
D O I：
10.1107/S160053681002934X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C21H23N3O4, the pyrazole ring forms dihedral angles of 21.58 (8) and 66.64 (7)degrees with the benzene and phenyl rings, respectively. The crystal structure is stabilized by weak intermolecular C-H...O hydrogen bonds.
引用
收藏
页码：O2149 / U2363
页数：11
相关论文
共 50 条
  • [1] (E)-4-[2-(4-chlorobenzyloxy)benzylideneamino]-1,5-dimethyl-2-phenyl-1H- pyrazol-3(2H)-one
    Zhang, Qiao-Zhen
    Zhao, Yan-Li
    Chen, Xin
    Yu, Ming
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O5252 - O5254
  • [2] 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
    Liang, Qiang
    Wang, Qian
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1968 - U766
  • [3] 4-[(E)-3-Methoxy-5-nitro-4-(4-nitrobenzyloxy)benzylideneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
    Liao, Lei
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2783 - U2290
  • [4] Experimental and DFT studies on the vibrational and electronic spectra of 1,5-dimethyl-2-phenyl-4-[(pyridin-4-ylmethylene)-amino]-1,2-dihydro-pyrazol-3-one
    Zhang, Yu
    Zhao, Jianying
    Li, Rongqing
    Jiang, Zhengjing
    Tang, Guodong
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2010, 77 (04) : 732 - 739
  • [5] Spectral, antimicrobial and anticancer activity of E-4-{[(5-bromothiophen-2-yl)methylidene]amino}-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
    Sasikala, M.
    Selvan, A.
    Nagaraja, K. S.
    Anuradha, R.
    Chandran, Karnan
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 2022, 738 (01) : 91 - 105
  • [6] Crystal structure of catena-poly[dichlorido-(μ2-1,5-dimethyl-2-phenyl-4-((pyridin-4-ylmethylene)amino)-1,2-dihydro-3H-pyrazol-3-one-κ2N:O) cobalt(II)] - methanol (1/1), C18H20Cl2CoN4O2
    Pang, Haixia
    Zou, Xiaoqing
    Tao, Defu
    Li, Jun
    Zhang, Jiahui
    Zhang, Hong
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (01): : 125 - 126
  • [7] Crystal structure of catena-poly[diiodido-(μ2-1,5-dimethyl-2-phenyl-4-((pyridin-3-ylmethylene)amino)-1,2-dihydro-3H-pyrazol-3-one-κ2N:O) zinc(II)], C17H16I2N4OZn
    Zhang, Hong
    Zou, Xiaoqing
    Feng, Qiran
    Xu, Baoming
    Pang, Haixia
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (06): : 1061 - 1062
  • [8] Single crystal XRD and DFT investigation of 1,5-dimethyl-4-[(2-oxo-1,2--diphenylethylidene) amino]-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
    Raj, S. Anila
    Vidya, V. G.
    Preethi, V.
    Kumar, V. G. Viju
    RESULTS IN CHEMISTRY, 2022, 4
  • [9] Synthesis and structure of 4-{[(E)-(7-methoxy-1,3-benzodioxol-5-yl)methylidene]amino}-1,5-dimethyl-2-phenyl-2,3-dihydro-1H-pyrazol-3-one
    Arderne, Charmaine
    Fotsing, Marthe Carine Djuide
    Ndinteh, Derek Tantoh
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2021, 77 : 200 - +
  • [10] 1-(4-Chlorophenyl)-3-phenyl-1H-pyrazol-5(4H)-one
    Ding, Yong-Jie
    Zhao, Chun-Xiang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O709 - U5797
12345