Modification of glassy carbon electrode by the electrochemical oxidation of 3-aminophenylcalix[4]pyrrole in nonaqueous media

被引：9
作者：
Taner, Bilge [2 ]
Deveci, Pervin [2 ]
Ustundag, Zafer [3 ]
Keskin, Selda [4 ]
Ozcan, Emine [2 ]
Solak, Ali Osman [1 ,5 ]
机构：
[1] Ankara Univ, Fac Sci, Dept Chem, TR-06100 Ankara, Turkey
[2] Selcuk Univ, Fac Sci, Dept Chem, Konya, Turkey
[3] Dumlupinar Univ, Fac Arts & Sci, Dept Chem, Kutahya, Turkey
[4] Middle E Tech Univ, Cent Res Lab, TR-06531 Ankara, Turkey
[5] Kyrgyz Turkish Manas Univ, Fac Eng, Dep Chem, Bishkek, Kyrgyzstan
来源：
SURFACE AND INTERFACE ANALYSIS | 2012年 / 44卷 / 02期
关键词：
calix[4]pyrrole; glassy carbon electrode; electrochemical oxidation; surface characterization; X-ray photoelectron spectroscopy; atomic force microscopy; ANION; SURFACES; BINDING; CHEMISTRY; FILMS; XPS; AFM;
D O I：
10.1002/sia.3794
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
3-Aminophenylcalix[4]pyrrole (3APCP) was grafted to a glassy carbon (GC) surface during the electrochemical oxidation process in 0.1 M tetrabutylammoniumtetra-fluoroborate (TBATFB) containing acetonitrile solution. The presence of a surface film was confirmed electrochemically by comparing voltammograms of dopamine and ferricyanide redox probes at the bare and modified electrodes. Reflection-absorption infrared spectroscopy (RAIRS), XPS, atomic force microscopy (AFM), ellipsometry and the contact angle measurements were also employed to characterize 3APCP film on GC electrode. RAIRS analysis revealed that calix[4]pyrrole was bonded to the glassy carbon surface via the etheric linkage. The stability of the modified GC electrode was also studied. Copyright (C) 2011 John Wiley & Sons, Ltd.
引用
收藏
页码：185 / 191
页数：7
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