Sonochemical Synthesis and Characterization of Copper Oxide Nanoparticles

被引：86

作者：

Wongpisutpaisan, Narongdet ^{[1
]}

Charoonsuk, Piyanut ^{[1
]}

Vittayakorn, Naratip ^{[1
]}

Pecharapa, Wisanu ^{[1
]}

机构：

[1] King Mongkuts Inst Technol Ladkrabang, Coll KMITL Nanotechnol, Bangkok 10520, Thailand

来源：

9TH ECO-ENERGY AND MATERIALS SCIENCE AND ENGINEERING SYMPOSIUM | 2011年 / 9卷

关键词：

Copper oxide; sonochemical; polyvinyl alcohol; CUO;

D O I：

10.1016/j.egypro.2011.09.044

中图分类号：

TE [石油、天然气工业]; TK [能源与动力工程];

学科分类号：

0807 ; 0820 ;

摘要：

Copper oxide (CuO) nanoparticles were synthesized by a sonochemical process using copper nitrate and sodium hydroxide in the presence of polyvinyl alcohol (PVA) as a starting precursor. The precipitated product was calcined at various temperature ranging from 400-700 degrees C. The physical microstructure and morphology of as-calcined nanoparticles were characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). From XRD observation, it is evident that the high purity CuO nanoparticles were obtained by this synthesis process. It was additionally revealed that its crystallization and particle size was strongly dependent on the reaction time and calcination temperature. (C) 2011 Published by Elsevier Ltd. Selection and/or peer-review under responsibility of CEO of Sustainable Energy System, Rajamangala University of Technology Thanyaburi (RMUTT).

引用

页数：6

共 15 条

[1] Controlled growth and characteristics of single-phase Cu2O and CuO films by pulsed laser deposition [J].

Chen, Aiping ;

Long, Hua ;

Li, Xiangcheng ;

Li, Yuhua ;

Yang, Guang ;

Lu, Peixiang .

VACUUM, 2009, 83 (06) :927-930

[2] Electrical and CO gas sensing properties of layered ZnO-CuO sensor [J].

Choi, JD ;

Choi, GM .

SENSORS AND ACTUATORS B-CHEMICAL, 2000, 69 (1-2) :120-126

[3]

Deng Chonghai, 2011, ULTRASONICS IN PRESS

[4] Spectroellipsometric characterization of sol-gel TiO2-CuO thin coatings [J].

Gartner, M ;

Scurtu, R ;

Ghita, A ;

Zaharescu, M ;

Modreanu, M ;

Trapalis, C ;

Kokkoris, M ;

Kordas, G .

THIN SOLID FILMS, 2004, 455 :417-421

[5]

Gartner M., 2004, THIN SOLID FILMS, P455

[6] Ultrasound induced cavitation and sonochemical yields [J].

Gong, CL ;

Hart, DP .

JOURNAL OF THE ACOUSTICAL SOCIETY OF AMERICA, 1998, 104 (05) :2675-2682

[7] Preparation of shape-controlled copper oxide powders from copper-containing solution [J].

Kim, YK ;

Riu, DH ;

Kim, SR ;

Kim, BI .

MATERIALS LETTERS, 2002, 54 (2-3) :229-237

[8] Sonochemical preparation and characterization of nanocrystalline copper oxide embedded in poly(vinyl alcohol) and its effect on crystal growth of copper oxide [J].

Kumar, RV ;

Elgamiel, R ;

Diamant, Y ;

Gedanken, A ;

Norwig, J .

LANGMUIR, 2001, 17 (05) :1406-1410

[9] A novel CuO-nanotube/SnO2 composite as the anode material for lithium ion batteries [J].

Li, Chao ;

Wei, Wei ;

Fang, Shaoming ;

Wang, Huanxin ;

Zhang, Yong ;

Gui, Yanghai ;

Chen, Rongfeng .

JOURNAL OF POWER SOURCES, 2010, 195 (09) :2939-2944

[10] Versatile synthesis of rectangular shaped nanobat-like CuO nanostructures by hydrothermal method; structural properties and growth mechanism [J].

Li, Fei ;

Tao, Kong ;

Wentuan, Bi ;

Li, Dachang ;

Li, Zhen ;

Huang, Xintang .

APPLIED SURFACE SCIENCE, 2009, 255 (12) :6279-6284

← 1 2 →