Synthesis and characterisation of macrocycles containing both tetrazole and pyridine functionalities

被引：15

作者：

Fleming, Adrienne ^{[2
]}

Gaire, Jackie ^{[2
]}

Kelleher, Fintan ^{[2
]}

McGinley, John ^{[1
]}

Mckee, Vickie ^{[3
]}

机构：

[1] Natl Univ Ireland Maynooth, Dept Chem, Maynooth, Co Kildare, Ireland

[2] Inst Technol Tallaght, Mol Design & Synth Grp, Dept Sci, Dublin 24, Ireland

[3] Univ Loughborough, Dept Chem, Loughborough LE11 3TU, Leics, England

来源：

TETRAHEDRON | 2011年 / 67卷 / 18期

关键词：

Tetrazole; Macrocycles; Pyridine; Synthesis; X-ray structure; COORDINATION POLYMERS; NITRILES; SALTS; WATER; AZIDE;

D O I：

10.1016/j.tet.2011.02.080

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The syntheses of tetra-tetrazole macrocycles containing at least one 2,6-bis(tetrazole)pyridine unit, linked by a variety of n-alkyl (n=3, 5, 7 or 9 carbon atoms) chain lengths, are described. There has been no previous incorporation of the pyridine moiety into a tetra-tetrazolophane macrocycle. The crystal structure of one such tetra-tetrazole macrocycle has also been structurally characterised and revealed a bowl-shaped conformation. (C) 2011 Elsevier Ltd. All rights reserved.

引用

页码：3260 / 3266

页数：7

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