Synthesis and characterisation of macrocycles containing both tetrazole and pyridine functionalities

被引：15
|
作者：
Fleming, Adrienne [2 ]
Gaire, Jackie [2 ]
Kelleher, Fintan [2 ]
McGinley, John [1 ]
Mckee, Vickie [3 ]
机构：
[1] Natl Univ Ireland Maynooth, Dept Chem, Maynooth, Co Kildare, Ireland
[2] Inst Technol Tallaght, Mol Design & Synth Grp, Dept Sci, Dublin 24, Ireland
[3] Univ Loughborough, Dept Chem, Loughborough LE11 3TU, Leics, England
来源：
TETRAHEDRON | 2011年 / 67卷 / 18期
关键词：
Tetrazole; Macrocycles; Pyridine; Synthesis; X-ray structure; COORDINATION POLYMERS; NITRILES; SALTS; WATER; AZIDE;
D O I：
10.1016/j.tet.2011.02.080
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The syntheses of tetra-tetrazole macrocycles containing at least one 2,6-bis(tetrazole)pyridine unit, linked by a variety of n-alkyl (n=3, 5, 7 or 9 carbon atoms) chain lengths, are described. There has been no previous incorporation of the pyridine moiety into a tetra-tetrazolophane macrocycle. The crystal structure of one such tetra-tetrazole macrocycle has also been structurally characterised and revealed a bowl-shaped conformation. (C) 2011 Elsevier Ltd. All rights reserved.
引用
收藏
页码：3260 / 3266
页数：7
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