Preparation and characterization of tin sulfide films with or without sodium chloride

被引：6

作者：

Bronusiene, A. ^{[1
]}

Popov, A. ^{[2
]}

Ivanauskas, R. ^{[1
]}

Ancutiene, I ^{[1
]}

机构：

[1] Kaunas Univ Technol, Dept Phys & Inorgan Chem, Radvilenu Str 19, LT-50254 Kaunas, Lithuania

[2] Vilnius Univ, Ctr Nanotechnol & Mat Sci, Naugarduko Str 24, LT-03225 Vilnius, Lithuania

来源：

CHEMICAL PHYSICS | 2020年 / 535卷

关键词：

SILAR; Tin sulfide; FTO glass; Sodium chloride; SNS THIN-FILMS; OPTICAL-PROPERTIES; SOLAR-CELL; THERMOELECTRIC PROPERTIES; DEPOSITION; PHASE; FABRICATION; GROWTH; LAYER;

D O I：

10.1016/j.chemphys.2020.110766

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

The successive ionic adsorption and reaction (SILAR) method was used to obtain tin sulfide film on FTO glass. In this work tin sulfide films were prepared with or without the immersion stage in distilled water. As-deposited tin sulfide films consisted of orthorhombic structures SnS and Sn2S3. This multiphase composition of obtained thin films was confirmed by X-ray diffraction and Raman spectroscopy. The estimated average crystallite size was in the range of 14-31 nm and was dependent on the conditions of the film preparation. Energy-dispersive X-ray analysis showed that tin sulfides films prepared without the immersion stage in distilled water formed with sodium chloride. The percentage incorporation of sodium and chlorine in those films was 5.29-8.10 and 8.71-11.22 at. %, respectively. The addition of sodium and chlorine atoms exhibited better crystallinity and effected on the optical properties of tin sulfides films.

引用

页数：8

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