Synthesis of TiO2 rutile nanoparticles by PLA in solution

被引:10
作者
Caratto, V. [1 ,2 ]
Ferretti, M. [1 ,2 ]
Setti, L. [1 ,2 ]
机构
[1] Univ Genoa, Dipartimento Chim & Chim Ind, I-16146 Genoa, Italy
[2] CNR SPIN, I-16152 Genoa, Italy
关键词
TiO2; Rutile; Lasis; Nanoparticle; THIN-FILMS; PHASE-STABILITY; TEMPERATURE; MORPHOLOGY;
D O I
10.1016/j.apsusc.2011.10.057
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
This paper describes the synthesis of TiO2 nanoparticles by laser ablation in solution synthesis (Lasis). The laser excimer beam passes through a focusing lens and it is sent to the reaction chamber. The frequency used during the synthesis was 20 Hz, intensity 26 kV The metal ablated by the laser beam undergoes an oxidation process resulting from the reaction with water. We obtain TiO2 nanoparticles with average size of 6.5 nm, crystallized in the rutile structure. The crystallographic and morphological structure was studied by transmission electron microscopy. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:2393 / 2396
页数:4
相关论文
共 50 条
[31]   Effect of annealing on TiO2 nanoparticles [J].
Sugapriya, S. ;
Sriram, R. ;
Lakshmi, S. .
OPTIK, 2013, 124 (21) :4971-4975
[32]   Synthesis of TiO2 nanoparticles out of fluoride solutions [J].
Sofronov, Dmitry ;
Rucki, Miroslaw ;
Doroshenko, Andrii ;
Shaposhnyk, Anna ;
Kapustnik, Oleksii ;
Mateychenko, Pavel ;
Baumer, Vyacheslav ;
Zurowski, Wojciech .
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T, 2022, 17 :2267-2279
[33]   Synthesis and characterization of pure anatase TiO2 nanoparticles [J].
B. S. Shirke ;
P. V. Korake ;
P. P. Hankare ;
S. R. Bamane ;
K. M. Garadkar .
Journal of Materials Science: Materials in Electronics, 2011, 22 :821-824
[34]   Synthesis of TiO2 nanoparticles in a spinning disc reactor [J].
Mohammadi, Somaieh ;
Harvey, Adam ;
Boodhoo, Kamelia V. K. .
CHEMICAL ENGINEERING JOURNAL, 2014, 258 :171-184
[35]   Synthesis and characterization of pure anatase TiO2 nanoparticles [J].
Shirke, B. S. ;
Korake, P. V. ;
Hankare, P. P. ;
Bamane, S. R. ;
Garadkar, K. M. .
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2011, 22 (07) :821-824
[36]   Synthesis and Characterization of TiO2 Nanoparticles [J].
Liu, Ziquan ;
Wang, Ruming ;
Kan, Fangjun ;
Jiang, Fuyi .
ASIAN JOURNAL OF CHEMISTRY, 2014, 26 (03) :655-659
[37]   Investigation of photocatalytic properties of TiO2 nanoparticles belonging to rutile phase [J].
Gadirova, Elmina ;
Hajiyeva, Sevinj ;
Sujayev, Afsun .
JOURNAL OF MOLECULAR STRUCTURE, 2021, 1227
[38]   Room Temperature Synthesis of Rutile TiO2 and Its Application in Dye-Sensitized Solar Cells [J].
Liu Jia ;
Yang Hao-Tian ;
Zhang Jing-Bo ;
Zhou Xiao-Wen ;
Lin Yuan .
ACTA PHYSICO-CHIMICA SINICA, 2011, 27 (02) :408-412
[39]   Green synthesis and dye-sensitized solar cell application of rutile and anatase TiO2 nanorods [J].
Ekar, Satish U. ;
Shekhar, Ganga ;
Khollam, Yogesh B. ;
Wani, Poonam N. ;
Jadkar, Sandesh R. ;
Naushad, Mu ;
Chaskar, Manohar G. ;
Jadhav, Santosh S. ;
Fadel, Alaa ;
Jadhav, Vijaykumar V. ;
Shendkar, Janardhan H. ;
Mane, Rajaram S. .
JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2017, 21 (09) :2713-2718
[40]   Effect of TiO2 nanoparticles on the long-term hydrolytic degradation behavior of PLA [J].
Luo, Yan-Bing ;
Wang, Xiu-Li ;
Wang, Yu-Zhong .
POLYMER DEGRADATION AND STABILITY, 2012, 97 (05) :721-728