Elution of monomer from different bulk fill dental composite resins

被引:85
作者
Cebe, Mehmet Ata [1 ]
Cebe, Fatma [1 ]
Cengiz, Mehmet Fatih [2 ]
Cetin, Ali Riza [3 ]
Arpag, Osman Fatih [4 ]
Ozturk, Bora [3 ]
机构
[1] Abant Izzet Baysal Univ, Fac Dent, Dept Restorat Dent, Bolu, Turkey
[2] Akdeniz Univ, Food Safety & Agr Res Ctr, TR-07058 Antalya, Turkey
[3] Selcuk Univ, Fac Dent, Dept Restorat Dent, Konya, Turkey
[4] Mustafa Kemal Univ, Fac Dent, Dept Periodontol, Antakya, Turkey
关键词
Bulk fill composite resin; Elution; Residual monomer; HPLC; HUMAN GINGIVAL FIBROBLASTS; RESIDUAL MONOMERS; CUSPAL DEFLECTION; IN-VITRO; BIS-GMA; BASE MATERIALS; PULP CELLS; CONVERSION; COMPONENTS; DIMETHACRYLATE;
D O I
10.1016/j.dental.2015.04.008
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
Objective. The purpose of this study was to evaluate the elution of Bis-GMA, TEGDMA, HEMA, and Bis-EMA monomers from six bulk fill composite resins over four different time periods, using HPLC. Methods. Six different composite resin materials were used in the present study: Tetric Evo Ceram Bulk Fill (Ivoclar Vivadent, Amherst, NY), X-tra Fill (VOCO, Cuxhaven, Germany), Sonic Fill (Kerr, Orange, CA, USA), Filtek Bulk Fill (3M ESPE Dental Product, St. Paul, MN), SDR (Dentsply, Konstanz, Germany), EQUIA (GC America INC, Alsip, IL). The samples (4 mm thickness, 5 mm diameter) were prepared and polymerized for 20s with a light emitted diode unit. After fabrication, each sample was immediately immersed in 75 wt% ethanol/water solution used as extraction fluid and stored in the amber colored bottles at room temperature. Ethanol/water samples were taken (0.5 mL) at predefined time intervals:10 m (T1), 1 h (T2), 24h (T3) and 30 days (T4). These samples were analyzed by HPLC. The obtained data were analyzed with one-way ANOVA and Tukey HSD at significance level of p < 0.05. Results. Amount of eluted Bis-EMA and Bis-GMA from Tetric Evo Ceram Bulk Fill and amount of eluted TEGDMA and HEMA from X-tra Fill higher than others composites (p < 0.05). Significance. Residual monomers were eluted from bulk fill composite resins in all time periods and the amount of eluted monomers was increased with time. (C) 2015 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:E141 / E149
页数:9
相关论文
共 53 条
[1]   Post-cure depth of cure of bulk fill dental resin-composites [J].
Alrahlah, A. ;
Silikas, N. ;
Watts, D. C. .
DENTAL MATERIALS, 2014, 30 (02) :149-154
[2]   Degree of conversion of bulk-fill compared to conventional resin-composites at two time intervals [J].
Alshali, Ruwaida Z. ;
Silikas, Nick ;
Satterthwaite, Julian D. .
DENTAL MATERIALS, 2013, 29 (09) :E213-E217
[3]  
Altintas S. H., 2012, EUR J DENT, V6, P255
[4]  
[Anonymous], 1988, REC CHEM DAT IND FOO
[5]   Pattern of cell death after in vitro exposure to GDMA, TEGDMA, HEMA and two compomer extracts [J].
Becher, Rune ;
Molvig Kopperud, Hilde ;
Al, Ronald H. ;
Samuelsen, Jan Tore ;
Morisbak, Else ;
Dahlman, Hans Joergen ;
Lilleaas, Edel Marie ;
Dahl, Jon E. .
DENTAL MATERIALS, 2006, 22 (07) :630-640
[6]   Cuspal deflection and depth of cure in resin-based composite restorations filled by using bulk, incremental and transtooth-illumination techniques [J].
Campodonico, Carlos E. ;
Tantbirojn, Daranee ;
Olin, Paul S. ;
Versluis, Antheunis .
JOURNAL OF THE AMERICAN DENTAL ASSOCIATION, 2011, 142 (10) :1176-1182
[7]   Marginal adaptation of class II cavities restored with bulk-fill composites [J].
Campos, Edson Alves ;
Ardu, Stefano ;
Lefever, Dorien ;
Jasse, Fernanda Ferreira ;
Bortolotto, Tissiana ;
Krejci, Ivo .
JOURNAL OF DENTISTRY, 2014, 42 (05) :575-581
[8]   The effect of BisGMA on cyclooxygenase-2 expression, PGE2 production and cytotoxicity via reactive oxygen species- and MEK/ERK-dependent and -independent pathways [J].
Chang, Mei-Chi ;
Lin, Li-Deh ;
Chan, Chiu-Po ;
Chang, Hsiao-Hua ;
Chen, Lin-I ;
Lin, Hsueh Jen ;
Yeh, Hung-Wei ;
Tseng, Wan Yu ;
Lin, Po-Shuen ;
Lin, Chiu-Chun ;
Jeng, Jiiang-Huei .
BIOMATERIALS, 2009, 30 (25) :4070-4077
[9]   The effects of BIS-GMA and TEG-DMA on female mouse fertility [J].
Darmani, H ;
Al-Hiyasat, AS .
DENTAL MATERIALS, 2006, 22 (04) :353-358
[10]   Influence of Degree of Conversion on the Biocompatibility of Different Composites In Vivo [J].
dos Santos, Rogerio Lacerda ;
de Morals Sannpaio, Geisa Aiane ;
de Carvalho, Fabiola Galbiatti ;
Pithon, Matheus Melo ;
Tenorio Guenes, Gynnenna Maria ;
Alves, Polliana Muniz .
JOURNAL OF ADHESIVE DENTISTRY, 2014, 16 (01) :15-20