The evaluation of nickel deposit obtained via Watts electrolyte at ambient temperature

被引:22
作者
Badarulzaman, Nur Azam [2 ]
Mohamad, Ahmad Azmin [1 ]
Puwadaria, Sunara [1 ]
Ahmad, Zainal Arifin [1 ]
机构
[1] Univ Sains Malaysia, Sch Mat & Minerals Resources Engn, Nibong Tebal 14300, Pulau Pinang, Malaysia
[2] Univ Tun Hussein Onn Malaysia, Fac Mech & Mfg Engn, Parit Raja 86400, Johor, Malaysia
关键词
Electroplating; Nickel electrodeposition; Watts electrolyte; Ambient temperature; COMPOSITE COATINGS; CURRENT-DENSITY; ELECTRODEPOSITION;
D O I
10.1007/s11998-010-9271-4
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A series of electroplating works were conducted to investigate the best conditions for the electrodeposition of nickel on a mild steel substrate. The electrodeposition was done at ambient electrolyte temperature with mild agitation and under current density ranging from 10 to 50 mA/cm(2). X-ray diffraction analysis (2 theta for first three peaks = 44.6, 51.9, and 76.8) and Energy Dispersive Spectrometer verified the presence of a pure nickel coating. Under field emission scanning electron microscopy analysis, the coating shows a typical nodular surface morphology, while cross-sectional microstructures show a compact nickel layer. Vickers hardness testing shows that the coating hardness gave the highest value of 293 HV at 30 mA/cm(2) current density.
引用
收藏
页码:815 / 820
页数:6
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