A novel method for PAHs in aqueous samples based on ultrasound-assisted solidified floating organic drop microextraction

被引：2
作者：
Song, Xiaofang [1 ]
Zhang, Shenghan [1 ]
Li, Tingting [1 ]
机构：
[1] North China Elect Power Univ, Sch Environm Sci & Engn, Baoding 071003, Hebei, Peoples R China
来源：
INTERNATIONAL CONFERENCE ON ENERGY ENGINEERING AND ENVIRONMENTAL PROTECTION (EEEP2017) | 2018年 / 121卷
关键词：
LIQUID-LIQUID MICROEXTRACTION; GAS-CHROMATOGRAPHY; PESTICIDES; POLLUTANTS;
D O I：
10.1088/1755-1315/121/2/022017
中图分类号：
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号：
0807 ; 0820 ;
摘要：
A novel method for determining PAHs in river samples has been developed based on ultrasound-assisted solidified floating organic drop microextraction. The effect of several factors, such as volume of extracting solvent, volume of aqueous sample, sample temperature and extraction time, were evaluated and optimized. Best enrichment efficiency was obtained under the following experimental conditions: 60 mu L of 1-undecanol added into a 30 mL sample solution at 40 degrees C, and then extracted for 10 min in an ultrasonic bath. It showed a good performance for determining the PAHs in river samples and will be a promising method for the reliable determination of PAHs at a very low level in river.
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页数：7
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