Synthesis of nanocrystalline Mn3O4 at 100 °C

被引：56
作者：
Anilkumar, M
Ravi, V
机构：
[1] Natl Chem Lab, Phys & Mat Chem Div, Pune 411008, Maharashtra, India
[2] Natl Chem Lab, Catalysis Div, Pune 411008, Maharashtra, India
来源：
MATERIALS RESEARCH BULLETIN | 2005年 / 40卷 / 04期
关键词：
ceramics; oxides; chemical synthesis; X-ray diffraction; electron microscopy;
D O I：
10.1016/j.materresbull.2005.01.009
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A simple gel to crystal conversion route has been followed for the preparation of nanocrystalline tetragonal Mn3O4 powders at 80-100 degrees C under refluxing conditions. Freshly prepared manganese hydroxide gel is allowed to crystallize under refluxing and stirring conditions for 4-6 h. Formation of nano crystallites of Mn3O4 is confirmed by X-ray diffraction (XRD) study. Transmission electron microscope (TEM) investigations revealed that the average particle size is 50 nm for these powders. (c) 2005 Elsevier Ltd. All rights reserved.
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收藏
页码：605 / 609
页数：5
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