Quantitative NIR determination of isoflavone and saponin content of ground soybeans

被引:43
作者
Berhow, Mark A. [1 ]
Singh, Mukti [1 ]
Bowman, Michael J. [2 ]
Price, Neil P. J. [3 ]
Vaughn, Steven F. [1 ]
Liu, Sean X. [1 ]
机构
[1] ARS, Funct Foods Res Unit, USDA, Natl Ctr Agr Utilizat Res, 1815 N Univ St, Peoria, IL 61604 USA
[2] ARS, Bioenergy Res Unit, USDA, Natl Ctr Agr Utilizat Res, 1815 N Univ St, Peoria, IL 61604 USA
[3] ARS, Renewable Prod Technol Res Unit, USDA, Natl Ctr Agr Utilizat Res, 1815 N Univ St, Peoria, IL 61604 USA
关键词
Near infrared spectrometry; Analysis; Soybean; Isoflavones; Saponins; Carbohydrates; Composition; INFRARED REFLECTANCE SPECTROSCOPY; GLYCINE-MAX; SUCROSE CONTENT; FATTY-ACIDS; SOY; SEED; SOYASAPONINS; EXTRACTION; CULTIVARS; PRODUCTS;
D O I
10.1016/j.foodchem.2020.126373
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Over 3200 discrete soybean samples were obtained from production locations around the United States during the years 2012-2016. Ground samples were scanned on near infrared spectrometers (NIRS) and analyzed by HPLC for total isoflavone and total saponin composition, as well as total carbohydrate composition. Multiple Linear Regression (MLR) analysis of preprocessed spectral data was used to develop optimized models to predict isoflavone content. The selection of a suitable calibration model was based on a high regression coefficient (R-2), and lower standard error of calibration (SEC) values. Robust validated predictions were obtained for isoflavones, however less than robust calibrations were obtained for the total saponins. The correlations were not as robust for predicting the carbohydrate composition. NIRS is a suitable, rapid, nondestructive method to determine isoflavone composition in ground soybeans. Useful isoflavone composition predictions for large numbers of soybean samples can be obtained from quickly obtained NIRS scans.
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页数:9
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共 40 条
[11]   Composition and characterization of soyabean and related products [J].
Garcia, MC ;
Torre, M ;
Marina, ML ;
Laborda, F .
CRITICAL REVIEWS IN FOOD SCIENCE AND NUTRITION, 1997, 37 (04) :361-391
[12]  
Gould K. S., 2006, Flavonoids: chemistry, biochemistry and applications, P397
[13]   Improved methods for the extraction and analysis of isoflavones from soy-containing foods and nutritional supplements by reversed-phase high-performance liquid chromatography and liquid chromatography-mass spectrometry [J].
Griffith, AP ;
Collison, MW .
JOURNAL OF CHROMATOGRAPHY A, 2001, 913 (1-2) :397-413
[14]   Non-destructive Determination of High Oleic Acid Content in Single Soybean Seeds by Near Infrared Reflectance Spectroscopy [J].
Han, Sang-Ik ;
Chae, Jong-Hyun ;
Bilyeu, Kristin ;
Shannon, J. Grover ;
Lee, Jeong-Dong .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 2014, 91 (02) :229-234
[15]   Evaluation of nonstarch polysaccharides and oligosaccharide content of different soybean varieties (Glycine max) by near-infrared spectroscopy and proteomics [J].
Hollung, K ;
Overland, M ;
Hrustic, M ;
Sekulic, P ;
Miladinovic, J ;
Martens, H ;
Narum, B ;
Sahlstrom, S ;
Sorensen, M ;
Storebakken, T ;
Skrede, A .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2005, 53 (23) :9112-9121
[16]   Standardisation of near infrared spectrometers: evaluation of some common techniques for intra- and inter-brand calibration transfer [J].
Igne, Benoit ;
Hurburgh, Charles R., Jr. .
JOURNAL OF NEAR INFRARED SPECTROSCOPY, 2008, 16 (06) :539-550
[17]   Chemical and nutritional properties of soybean carbohydrates as related to nonruminants: A review [J].
Karr-Lilienthal, LK ;
Kadzere, CT ;
Grieshop, CM ;
Fahey, GC .
LIVESTOCK PRODUCTION SCIENCE, 2005, 97 (01) :1-12
[18]   Comparison of isoflavones composition in seed, embryo, cotyledon and seed coat of cooked-with-rice and vegetable soybean (Glycine max L.) varieties [J].
Kim, Jin-Ae ;
Hong, Seung-Beom ;
Jung, Woo-Suk ;
Yu, Chang-Yeon ;
Ma, Kyung-Ho ;
Gwag, Jae-Goon ;
Chung, Ill-Min .
FOOD CHEMISTRY, 2007, 102 (03) :738-744
[19]   MALONYL ISOFLAVONE GLYCOSIDES IN SOYBEAN SEEDS (GLYCINE-MAX MERRILL) [J].
KUDOU, S ;
FLEURY, Y ;
WELTI, D ;
MAGNOLATO, D ;
UCHIDA, T ;
KITAMURA, K ;
OKUBO, K .
AGRICULTURAL AND BIOLOGICAL CHEMISTRY, 1991, 55 (09) :2227-2233
[20]   Variation in isoflavone of soybean cultivars with location and storage duration [J].
Lee, SJ ;
Ahn, JK ;
Kim, SH ;
Kim, JT ;
Han, SJ ;
Jung, MY ;
Chung, IM .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2003, 51 (11) :3382-3389