Dielectric properties of CaCu3Ti4O12 prepared by sol-gel self combustion technique

被引:25
|
作者
Kumar, C. [1 ]
机构
[1] Univ Madras, Dept Phys, LN Govt Coll, Ponneri 601204, Tamil Nadu, India
关键词
CERAMICS; MICROSTRUCTURE; CONSTANTS;
D O I
10.1007/s10854-010-0179-7
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
The preparation of Calcium copper titanate (CCTO) nanopowder was carried out by a sol-gel self combustion method. The X-ray diffraction analysis indicated that the samples calcined at 800 A degrees C were fully crystallized in the CCTO phase. The results of atomic force microscope showed the particles size of CCTO was in the range of 60-80 nm. The absorption bands corresponding to vibrations of Cu-O, Ti-O-Ti and nu Ca-O were observed at 512, 450 and 562 cm(-1) using FTIR. The samples sintered at 950 A degrees C showed the densities as high as 97% of theoretical density. The grain sizes of sintered pellets were determined by HRSEM. The dielectric properties of prepared samples were studied by LCR meter.
引用
收藏
页码:579 / 582
页数:4
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