Sol-gel preparation and properties of Ag-TiO2 films on surface roughened Ti-6Al-4V alloy

被引:23
作者
Fu, T. [1 ]
Shen, Y. G. [2 ]
Alajmi, Z. [1 ]
Yang, S. Y. [1 ]
Sun, J. M. [1 ]
Zhang, H. M. [1 ]
机构
[1] Xi An Jiao Tong Univ, Key Lab Biomed Informat Engn, Sch Life Sci & Technol, Minist Educ, Xian 710049, Peoples R China
[2] City Univ Hong Kong, Dept Mech & Biomed Engn, Kowloon, Hong Kong, Peoples R China
关键词
TiO2; Ag; Antibacterial; Sol-gel; Corrosion; TIO2; FILM; THIN-FILMS; ANTIBACTERIAL; COATINGS; TITANIUM; BIOCOMPATIBILITY; NANOPARTICLES; ADHESION;
D O I
10.1179/1743284714Y.0000000650
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Ag-TiO2 films (Ag/Ti=3.3, 9.1 at-%) were sol-gel coated on Ti-6Al-4V alloy that had been surface roughened by the NaOH-HCl treatment for antibacterial applications. Scanning electron microscopy observation showed that pore size of the surface layer of NaOH-HCl treated Ti-6Al- 4V alloy increased with the NaOH concentration. Ag-TiO2 films on the surface roughened substrate were adherent and crack-free. X-ray photoelectron spectroscopy and Auger electron spectroscopy analyses indicated that Ag existed in metallic state, and the films completely covered the roughened substrate. X-ray diffraction peaks of the substrate and anatase TiO2 were detected. The Ag-TiO2 films on the roughened substrate exhibited good adhesion quality and high cohesion strength in the indentation test. The potentiodynamic polarisation test showed that the TiO2 and Ag-TiO2 films improved corrosion resistance of the substrate.
引用
收藏
页码:501 / 505
页数:5
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