New Effective Synthetic Method for Preparation of N,N-Dichlorocarbamates

被引：4

作者：

Gutch, P. K. ^{[1
]}

Singh, Ravindra ^{[1
]}

Prabha, S. ^{[2
]}

Suryanarayana, M. V. S. ^{[1
]}

机构：

[1] Def Res & Dev Estab, Synthet Chem Div, Gwalior 474002, MP, India

[2] Jiwaji Univ, Sch Studies Chem, Gwalior 474011, India

来源：

SYNTHETIC COMMUNICATIONS | 2011年 / 41卷 / 10期

关键词：

Acidic medium; sodium hypochlorite; substituted N; N-dichlorocarbamates; SULFUR MUSTARD; SULFONAMIDE; OXIDATION; CHEMISTRY; EFFICACY; SIMULANT; SULFIDES;

D O I：

10.1080/00397911.2010.488311

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

[image omitted] A rapid, efficient, economical, and easy-to-scale method for the effective conversion of carbamates to corresponding N,N-dichlorocarbamates by using sodium hypochlorite in acidic medium has been described. N,N-Dichlorocarbamates were obtained in quantitative yield through a simple workup in reduced reaction time.

引用

页码：1554 / 1557

页数：4

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