Preparation and Properties of TiO2 Nanoparticles in situ Surface-modified with Salicylic Acid

被引:4
作者
Hu Bin [1 ]
Pan Hui [1 ]
Yu Lai-Gui [1 ]
Wang Long-Ge [2 ]
Zhao Lei [2 ]
Zhang Zhi-Jun [1 ]
机构
[1] Henan Univ, Key Lab Special Funct Mat, Kaifeng 475004, Peoples R China
[2] Henan Univ, Sch Phys, Kaifeng 475004, Peoples R China
关键词
TiO2; nanoparticles; salicylic acid; surface-modified; CARBOXYLIC-ACID; TITANIUM;
D O I
10.3724/SP.J.1077.2011.01181
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The surface of TiO2 nanoparticles prepared by controlling hydrolysis of a titanium tetrachloride (TiCl4) precursor was modified with salicylic acid (SA). The prepared samples were characterized by X-ray diffraction (XRD), high resolution transmission electron microscope (HRTEM) and Fourier transformation infrared spectrometry (FT-IR). The chemical feature and state of TiO2/SA were analyzed by X-ray photoelectron spectroscope (XPS). From the experiments, the surface-modified TiO2 nanoparticles with SA have excellent dispersibility in ethanol. As functionalized inorganic fillers, TiO2/SA nanoparticles increase the diffraction efficiency and reduce the Bragg mismatch of the photopolymer film, which have a great applied prospect in holographic data storage (HDS).
引用
收藏
页码:1181 / 1186
页数:6
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