Sonochemical synthesis of a nano-structured zinc(II) amidic pillar metal-organic framework

被引：35

作者：

Bigdeli, Mina ^{[1
]}

Morsali, Ali ^{[1
]}

机构：

[1] Tarbiat Modares Univ, Dept Chem, Fac Sci, Tehran, Iran

来源：

ULTRASONICS SONOCHEMISTRY | 2015年 / 27卷

关键词：

Metal-organic framework; Sonochemical; Amidic pillar; Nano-structure; COORDINATION POLYMER PRECURSOR; HYDROGEN; NANOSTRUCTURES; FABRICATION; ADSORPTION; NANOCRYSTALS; COMPLEXES;

D O I：

10.1016/j.ultsonch.2015.05.034

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

A facile and environmentally friendly nano-scale synthesis of a Zn(II) metal-organic framework (MOP), {[Zn-4(BDC)(4)(bpta)(4)]center dot 5DMF center dot 3H(2)O}(n) (1) (bpta = N,N'-bis(4-pyridinyl)-1,4-benzenedicarboxamide, BDC = 1,4-dicarboxylate, DMF = N,N-dimethylformamide), with nanorods morphology under ultrasonic irradiation at ambient temperature and atmospheric pressure has been explored. This MOF has been characterized by scanning electron microscopy (SEM), powder X-ray diffraction (PXRD) and IR spectroscopy. Some parameters such as concentration of initial reagents, power ultrasound irradiation and time effects on size and morphology of nano-structured compound 1 have been studied. (C) 2015 Elsevier B.V. All rights reserved.

引用

页码：416 / 422

页数：7

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