Microstructural, physical, and optical characterization of high-translucency zirconia ceramics

Statement of problem. The microstructural, physical, and optical properties of newly available highly-translucent zirconia ceramics have not been thoroughly investigated. Purpose. The purpose of this in vitro study was to evaluate the microstructural, physical, and optical properties of current zirconia ceramics with different degrees of translucency and to compare the optical properties with lithium disilicate glass-ceramic at different thicknesses. Material and methods. Disk-shaped specimens (N=108) were prepared from 3 different monolithic zirconia ceramics: VITA YZ HT (YZ-HT), VITA YZ ST (YZ-ST), and VITA YZ XT (YZ-XT) and lithium disilicate glass-ceramic (IPS e-max CAD LT [IPS]) with a diameter of 14 mm and 3 different thicknesses (0.5, 1.0, and 1.5 mm +/- 0.02 mm). The microstructural features (grain size, elemental composition, phase identifications, and quantifications), physical properties (Vickers hardness and fracture toughness), and optical properties (translucency parameter and contrast ratio) were investigated. Data were analyzed using 1-way ANOVA, followed by the post hoc Tukey tests or Kruskal-Wallis and Mann-Whitney U tests (alpha=.05). Results. Differences in grain size, phase assemblages, fracture toughness, translucency parameter, and contrast ratio were found to be significant (P<.05). The average grain size was different for the 3 zirconia specimens with the following order: YZ-XT>YZ-ST>YZ-HT. The fracture toughness of YZ-HT was higher than that of YZ-ST and YZ-XT (P<.05). IPS with 0.5-mm thickness had the highest TP followed by YZ-XT and YZ-ST. The CR values were in the range of 0.54 to 0.91 (YZ-HT), 0.43 to 0.61 (YZ-ST), 0.29 to 0.45 (YZ-XT), and 0.27 to 0.53 (IPS), and all decreased with an increase in thickness. Conclusions. Based on the results of the present study, the microstructural, physical, and optical properties of zirconia ceramics were affected by the changes in chemical composition and sintering parameters.