Structural characterization of biomedical Co-Cr-Mo components produced by direct metal laser sintering

被引:94
作者
Barucca, G. [1 ]
Santecchia, E. [1 ]
Majni, G. [1 ]
Girardin, E. [2 ]
Bassoli, E. [3 ]
Denti, L. [3 ]
Gatto, A. [3 ]
Iuliano, L. [4 ]
Moskalewicz, T. [5 ]
Mengucci, P. [1 ]
机构
[1] Univ Politecn Marche, SIMAU, I-60131 Ancona, Italy
[2] Univ Politecn Marche, DISCO, I-60131 Ancona, Italy
[3] Univ Modena & Reggio Emilia, DIMeC, I-41125 Modena, Italy
[4] Politecn Torino, DISPEA, I-10129 Turin, Italy
[5] AGH Univ Sci & Technol, Fac Met Engn & Ind Comp Sci, PL-30059 Krakow, Poland
来源
MATERIALS SCIENCE AND ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS | 2015年 / 48卷
关键词
Metals and alloys; Laser processing; Sintering; Transmission electron microscopy; TEM; Scanning electron microscopy; SEM; X-ray diffraction; MECHANICAL-PROPERTIES; MICROSTRUCTURE; IMPLANTS; ALLOYS;
D O I
10.1016/j.msec.2014.12.009
中图分类号
TB3 [工程材料学]; R318.08 [生物材料学];
学科分类号
0805 ; 080501 ; 080502 ;
摘要
Direct metal laser sintering (DMLS) is a technique to manufacture complex functional mechanical parts from a computer-aided design (CAD) model. Usually, the mechanical components produced by this procedure show higher residual porosity and poorer mechanical properties than those obtained by conventional manufacturing techniques. In this work, a Co-Cr-Mo alloy produced by DMLS with a composition suitable for biomedical applications was submitted to hardness measurements and structural characterization. The alloy showed a hardness value remarkably higher than those commonly obtained for the same cast or wrought alloys. In order to clarify the origin of this unexpected result, the sample microstructure was investigated by X-ray diffraction (XRD), electron microscopy (SEM and TEM) and energy dispersive microanalysis (EDX). For the first time, a homogeneous microstructure comprised of an intricate network of thin a (hcp)-lamellae distributed inside a gamma (fcc) phase was observed. The e-lamellae grown on the {111}gamma planes limit the dislocation slip inside the gamma (fcc) phase, causing the measured hardness increase. The results suggest possible innovative applications of the DMLS technique to the production of mechanical parts in the medical and dental fields. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:263 / 269
页数:7
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