A sensitive nonenzymatic hydrogen peroxide sensor based on Fe3O4-Fe2O3 nanocomposites

被引:21
作者
Cao, Guang Sheng [1 ]
Wang, Peilong [1 ]
Li, Xin [1 ]
Wang, Yue [1 ]
Wang, Guilong [1 ]
Li, Junping [1 ]
机构
[1] Northeast Petr Univ, Key Lab Enhanced Oil & Gas Recovery, Minist Educ, Daqing 163318, Peoples R China
关键词
Fe3O4; Fe2O3; nanocomposites; hydrogen peroxide; sensor; GLASSY-CARBON ELECTRODE; ELECTROCHEMICAL SENSOR; OXIDE NANOPARTICLES; REDUCTION; NANOTUBES; OXIDATION; H2O2;
D O I
10.1007/s12034-014-0803-x
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The Fe3O4-Fe2O3 nanocomposites were prepared by the co-precipitation method and followed by calcination process. The products were synthesized and characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and energy-dispersive X-ray analysis. The obtained Fe3O4-Fe2O3 nanocomposites were then applied to study the electrocatalytic reduction of hydrogen peroxide (H2O2) in 0.01 M pH 7.0 phosphate buffer medium. Then the Fe3O4-Fe2O3 nanocomposites were used as active electrode material of electrochemical sensors for H2O2 detection The detection sensitivity of the sensor was 20.325 mu A mM (-1) , and the detection limit was estimated to be about 0.2 mM.
引用
收藏
页码:163 / 167
页数:5
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