Comparative study of the Ag/PVP nanocomposites synthesized in water and in ethylene glycol

被引:16
作者
Arshi, Nishat [1 ]
Ahmed, Faheem [1 ]
Kumar, Shalendra [1 ]
Anwar, M. S. [1 ]
Koo, Bon Heun [1 ]
Lee, Chan Gyu [1 ]
机构
[1] Changwon Natl Univ, Sch Nano & Adv Mat Engn, Chang Won 641773, Gyeongnam, South Korea
关键词
Nanocomposites; Antibacterial activity; Escherichia coli; Silver nanoparticles; NANOPARTICLES; ANTIBACTERIAL;
D O I
10.1016/j.cap.2010.11.045
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
We report direct synthesis of Ag/PVP nanocomposites using PVP (polyvinylpyrrolidone) as a reducing agent. Ag/PVP nanocomposites were synthesized after mixing PVP with acetone and a small amount of aqueous silver nitrate (AgNO3) under magnetic stirring. The Ag/PVP colloids were then dissolved in water (sample 1) and in ethylene glycol (sample 2) and stirred for 10 days. UV/vis spectra show surface plasmon band in the visible region, centered at wavelengths between 435 and 445 nm, a clear consequence of the nano size of dilute Ag particles. TEM results showed that the Ag/PVP nanocomposites have particle sizes ranging from 1 to 6 nm and 1 to 12 nm for colloids in water and ethylene glycol respectively. Antibacterial activity of these silver nanocomposites as a function of particles concentration against gram-negative bacterium Escherichia coli (E. coli) was carried out in solid growth media. Both the nanocomposites showed good antibacterial activity and caused a growth delay of E. coli with zone of inhibition similar to 16 mm. There was very little difference between antibacterial activities of two types of silver nanocomposites, though sample 1 with smaller size showed a slightly better antibacterial action. (C) 2010 Elsevier B. V. All rights reserved.
引用
收藏
页码:S346 / S349
页数:4
相关论文
共 15 条
[1]   Chemistry and properties of nanocrystals of different shapes [J].
Burda, C ;
Chen, XB ;
Narayanan, R ;
El-Sayed, MA .
CHEMICAL REVIEWS, 2005, 105 (04) :1025-1102
[2]   Antibacterial and bioactive silver-containing Na2O • CaO • 2SiO2 glass prepared by sol-gel method [J].
Catauro, M ;
Raucci, MG ;
De Gaetano, F ;
Marotta, A .
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN MEDICINE, 2004, 15 (07) :831-837
[3]  
Chen X., 2008, TOXICOL LETT, V1, P176
[4]   The study of antimicrobial activity and preservative effects of nanosilver ingredient [J].
Cho, KH ;
Park, JE ;
Osaka, T ;
Park, SG .
ELECTROCHIMICA ACTA, 2005, 51 (05) :956-960
[5]   The preparation and characterization of silver-loading cellulose acetate hollow fiber membrane for water treatment [J].
Chou, WL ;
Yu, DG ;
Yang, MC .
POLYMERS FOR ADVANCED TECHNOLOGIES, 2005, 16 (08) :600-607
[6]  
Elechiguerra J.L., 2005, J NANOBIOTECHNOL, V3
[7]  
Klasen H J., 2000, Burns, V30, P1, DOI DOI 10.1016/S0305-4179(99)00108-4
[8]  
KOJARNOVITCH V, 1997, NEW ADV MAT EMERGING
[9]  
Mikihiro Y., 2005, APPL ENVIRON MICROB, V71, P7589
[10]   The bactericidal effect of silver nanoparticles [J].
Morones, JR ;
Elechiguerra, JL ;
Camacho, A ;
Holt, K ;
Kouri, JB ;
Ramírez, JT ;
Yacaman, MJ .
NANOTECHNOLOGY, 2005, 16 (10) :2346-2353