5-(4-Hydroxybenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

被引:5
作者
Zeng, Wu-Lan [1 ]
机构
[1] Weifang Univ, MicroScale Sci Inst, Dept Chem & Chem Engn, Weifang 261061, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
D O I
10.1107/S1600536810032149
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C(13)H(12)O(5), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 4-hydroxybenzaldehyde in ethanol. The 1,3-dioxane ring is in a distorted boat conformation. In the crystal, inversion dimers linked by pairs of O-H center dot center dot center dot O hydrogen bonds generate R(2)(2)(20) rings.
引用
收藏
页码:O2319 / U405
页数:8
相关论文
共 3 条
[1]  
Bruker, 1997, SMART SAINT
[2]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[3]   5-(2-Fluorobenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione [J].
Zeng, Wu-Lan ;
Jian, Fang-Fang .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O2587-+