Crystal structure of 1-(4,6-dimethylpyrimidin-2-yl)benzimidazole, C13H12N4

被引:0
作者
Li, Hong-Mei [2 ]
Xu, Chen [1 ]
Liu, Hu [2 ]
Zhang, Zhi-Qiang [2 ]
Yao, Jing-Cai [1 ]
Zhang, Yu-Qing [2 ]
机构
[1] Luoyang Normal Univ, Coll Chem & Chem Engn, Luoyang 471022, Peoples R China
[2] Henan Univ Sci & Technol, Sch Chem Engn & Pharmaceut, Luoyang 471003, Henan, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2011年 / 226卷 / 01期
关键词
N-HETEROCYCLIC CARBENES; COMPLEXES; NICKEL;
D O I
10.1524/ncrs.2011.0043
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C13H12N4, monoclinic, P12(1)/c 1 (no. 14), a = 8.682(1) angstrom, b = 17.542(3) angstrom, c = 7.571(1) angstrom, beta= 90.649(2)degrees, V = 1153.0 angstrom(3), Z = 4, R-gt(F)= 0.043, wR(ref)(F-2) = 0.111, T= 296 K.
引用
收藏
页码:89 / 90
页数:2
相关论文
共 9 条
[1]   MODEL SYSTEMS FOR TYPE-I COPPER PROTEINS - STRUCTURES OF COPPER COORDINATION-COMPOUNDS WITH THIOETHER AND AZOLE-CONTAINING LIGANDS [J].
BOUWMAN, E ;
DRIESSEN, WL ;
REEDIJK, J .
COORDINATION CHEMISTRY REVIEWS, 1990, 104 (01) :143-172
[2]   Heterocyclic carbenes: Synthesis and coordination chemistry [J].
Hahn, F. Ekkehardt ;
Jahnke, Mareike C. .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2008, 47 (17) :3122-3172
[3]   Palladium complexes of N-heterocyclic carbenes as catalysts for cross-coupling reactions - A synthetic chemist's perspective [J].
Kantchev, Eric Assen B. ;
O'Brien, Christopher J. ;
Organ, Michael G. .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2007, 46 (16) :2768-2813
[4]   Direct Synthesis of Iron, Cobalt, Nickel, and Copper Complexes of N-Heterocyclic Carbenes by Using Commercially Available Metal Powders [J].
Liu, Bin ;
Xia, Qinqin ;
Chen, Wanzhi .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2009, 48 (30) :5513-5516
[5]   SYNTHESIS, REACTIONS, AND SPECTROSCOPIC PROPERTIES OF BENZIMIDAZOLES [J].
PRESTON, PN .
CHEMICAL REVIEWS, 1974, 74 (03) :279-314
[6]  
Reedijk J., 1987, Comprehensive Coordination Chemistry: The Synthesis, Reactions, Properties and Applications of Coordination Compounds, V2
[7]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[8]   Synthesis and Structural Characterization of Monophosphine-Cyclopalladated Ferrocenylpyrimidine Complexes and Reusable Catalytic System for Amination of Hindered Aryl Chlorides in PEG-400 [J].
Xu, Chen ;
Wang, Zhi-Qiang ;
Fu, Wei-Jun ;
Lou, Xin-Hua ;
Li, Ying-Fei ;
Cen, Fei-Fei ;
Ma, Hong-Ji ;
Ji, Bao-Ming .
ORGANOMETALLICS, 2009, 28 (06) :1909-1916
[9]   Steric Bulkiness-Dependent Structural Diversity in Nickel(II) Complexes of N-Heterocyclic Carbenes: Synthesis and Structural Characterization of Tetra-, Penta-, and Hexacoordinate Nickel Complexes [J].
Zhang, Xiaoming ;
Lilu, Bin ;
Liu, Ailing ;
Xie, Weilong ;
Chen, Wanzhi .
ORGANOMETALLICS, 2009, 28 (05) :1336-1349