Determination of 241Am in sediments by isotope dilution high resolution inductively coupled plasma mass spectrometry (ID HR ICP-MS)

被引：29
|
作者：
Agarande, M [1 ]
Benzoubir, S [1 ]
Bouisset, P [1 ]
Calmet, D [1 ]
机构：
[1] Inst Nucl Safety & Protect, Environm Radioact Measurement Lab, F-91400 Orsay, France
来源：
APPLIED RADIATION AND ISOTOPES | 2001年 / 55卷 / 02期
关键词：
americium; sediments; ICP-MS;
D O I：
10.1016/S0969-8043(01)00045-8
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Trace levels (pg kg(-1)) of Am-241 in sediments were determined by isotope dilution high resolution inductively coupled plasma mass spectrometry (1D HR ICP-MS) using a microconcentric nebulizer. Am-241 was isolated from major elements like Ca and Fe by different selective precipitations. In Further steps, Am was first separated from other transuranic elements and purified by anion exchange and extraction chromatography prior to the mass spectrometric measurements. The ID HR ICP-MS results are compared with isotope dilution alpha spectrometry. (C) 2001 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：161 / 165
页数：5
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