Preparation of H-bar cross-sectional specimen for in situ TEM straining experiments: A FIB-based method applied to a nitrided Ti-6Al-4V alloy

被引:13
|
作者
Castany, P. [1 ,2 ]
Legros, M. [2 ]
机构
[1] INSA Rennes, UMR CNRS SCR Chim Met 6226, F-35708 Rennes 7, France
[2] CEMES CNRS, F-31055 Toulouse 4, France
来源
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 2011年 / 528卷 / 03期
关键词
In situ straining; Transmission electron microscopy (T'EM); Focused ion beam (FIB); Dislocation dynamics; Titanium alloy; Nitridation; THIN-FILMS; SINGLE-CRYSTAL; TITANIUM-ALLOY; DEFORMATION; MICROSCOPY; MECHANISMS; POLYIMIDE; BEHAVIOR; FRACTURE;
D O I
10.1016/j.msea.2010.10.025
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The in situ tensile straining of cross-sectional specimens inside a TEM is intrinsically very difficult to perform despite its obvious interest to study interfaces of surface treated materials. We have combined a FIB-based method to produce H-bar specimens of a nitrided Ti-6Al-4V alloy and in situ TEM straining stage, to successfully study the plastic deformation mechanisms that are activated close to the nitrided surface in the Ti-based alloy. (C) 2010 Elsevier B.V. All rights reserved.
引用
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页码:1367 / 1371
页数:5
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