Cerium doped magnetite nanoparticles for highly sensitive detection of metronidazole via chemiluminescence assay

被引：151
作者：
Orooji, Yasin [1 ,2 ]
Irani-nezhad, Mahsa Haddad [3 ]
Hassandoost, Ramin [3 ]
Khataee, Alireza [3 ,4 ,5 ]
Pouran, Shima Rahim [6 ]
Joo, Sang Woo [7 ]
机构：
[1] Nanjing Forestry Univ, Coll Mat Sci & Engn, 159 Longpan Rd, Nanjing 210037, Jiangsu, Peoples R China
[2] Nanjing Forestry Univ, Coinnovat Ctr Efficient Proc & Utilizat Forest Re, Nanjing 210037, Peoples R China
[3] Univ Tabriz, Fac Chem, Dept Appl Chem, Res Lab Adv Water & Wastewater Treatment Proc, Tabriz 5166616471, Iran
[4] Gebze Tech Univ, Dept Environm Engn, TR-41400 Gebze, Turkey
[5] Duy Tan Univ, Inst Res & Dev, Da Nang 550000, Vietnam
[6] Univ Mohaghegh Ardabili, Fac Sci, Dept Biol, POB 179, Ardebil, Iran
[7] Yeungnam Univ, Sch Mech Engn, Gyongsan 712749, South Korea
来源：
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY | 2020年 / 234卷
基金：
新加坡国家研究基金会;
关键词：
Antibiotics detection; Chemiluminescence; Human plasma; Magnetic sensor; Metronidazole; PERFORMANCE; SYSTEM; BIOSENSOR; ELECTRODE; FLUORESCENCE; LUMINESCENT; ADSORPTION; CATALYST; SAMPLES; WATER;
D O I：
10.1016/j.saa.2020.118272
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
Cerium doped magnetite nanoparticle (CDM) was synthesized via a co-precipitation method and used as the co-reactant of luminol-K3Fe(CN)(6) chemiluminescent system. The physical-chemical features of CDM were studied by XPS, XRD, HRTEM, FESEM, VSM, BET, and FTIR analyses. This simple and highly sensitive nanoprobe enabled the determination of minor concentrations of metronidazole (MNZ). Owing to the quenching efficacy of MNZ in the studied chemiluminescence system, a linear range of 3.47 x 10(-6)-9.37 x 10(-5) mol/L was obtained with a limit of detection of 3.91 x 10(-7) mol/L. This biosensor was used for MNZ detection in human serum samples, which was highly efficient. The outcomes of this study give credit to the proposed biosensor to be applied for detection of MNZ in biological samples. (C) 2020 Elsevier B.V. All rights reserved.
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页数：10
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