Effect of wall materials and core oil on the formation and properties of styralyl acetate microcapsules prepared by complex coacervation

被引:17
作者
Xiao, Zuobing [1 ]
Li, Wei [1 ]
Zhu, Guangyong [1 ]
机构
[1] Shanghai Inst Technol, Sch Perfume & Aroma Technol, Shanghai 201418, Peoples R China
关键词
Microcapsules; Response surface methodology; Complex coacervation; Styralyl acetate; Gelatin; Gum Arabic; SPHERICAL MULTINUCLEAR MICROCAPSULES; STRUCTURAL-PROPERTIES; MICROENCAPSULATION; GELATIN; GUM; RELEASE; PROTEIN; OPTIMIZATION; PARAMETERS;
D O I
10.1007/s00396-015-3515-x
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Styralyl acetate (SA) was encapsulated in gelatin and gum Arabic using complex coacervation. The response surface methodology was carried out to explore effects of wall concentration and the amount of SA on the yield, encapsulation efficiency, and oil loading capacity and to optimize the process conditions. The results of optimization showed that the wall concentration of 1.35 % (w/v) and the SA of 2.23 g were used, the highest yield of 72.8 %, encapsulation efficiency of 80.6 % and oil loading capacity of 66.2 % were obtained. The morphologies were observed by an optical microscope and scanning electron microscopy (SEM), respectively. Microcapsules exhibited excellent thermal stability than SA by thermogravimetric analysis (TGA). Moreover, Fourier transform infrared and X-ray diffraction examined structure changes of wall materials and core oil.
引用
收藏
页码:1339 / 1348
页数:10
相关论文
共 29 条
[1]   Photoluminescence and structural properties of CdSe quantum dot-gelatin composite films [J].
Borkovska, L. ;
Korsunska, N. ;
Stara, T. ;
Gudymenko, O. ;
Kladko, V. ;
Stroyuk, O. ;
Raevskaya, A. ;
Kryshtab, T. .
PHYSICA B-CONDENSED MATTER, 2014, 453 :86-91
[2]   Production of Turmeric Oleoresin Microcapsules by Complex Coacervation with Gelatin-Gum Arabic [J].
Cirelli Zuanon, Larissa Angelica ;
Malacrida, Cassia Roberta ;
Nicoletti Telis, Vania Regina .
JOURNAL OF FOOD PROCESS ENGINEERING, 2013, 36 (03) :364-373
[3]   Study of Complex Coacervation of Gelatin A with Sodium Carboxymethyl Cellulose: Microencapsulation of Neem (Azadirachta indica A. Juss.) Seed Oil (NSO) [J].
Devi, N. ;
Maji, T. K. .
INTERNATIONAL JOURNAL OF POLYMERIC MATERIALS, 2011, 60 (13) :1091-1105
[4]   Effect of processing parameters on the formation of spherical multinuclear microcapsules encapsulating peppermint oil by coacervation [J].
Dong, Z. J. ;
Toure, A. ;
Jia, C. S. ;
Zhang, X. M. ;
Xu, S. Y. .
JOURNAL OF MICROENCAPSULATION, 2007, 24 (07) :634-646
[5]   Optimization of cross-linking parameters during production of transglutaminase-hardened spherical multinuclear microcapsules by complex coacervation [J].
Dong, Zhi-Han ;
Xia, Shu-Qin ;
Hua, Serenus ;
Hayat, Khizar ;
Zhang, Xiao-Ming ;
Xu, Shi-Ying .
COLLOIDS AND SURFACES B-BIOINTERFACES, 2008, 63 (01) :41-47
[6]   Microencapsulation: industrial appraisal of existing technologies and trends [J].
Gouin, S .
TRENDS IN FOOD SCIENCE & TECHNOLOGY, 2004, 15 (7-8) :330-347
[7]   Preparation and Properties Analysis of Slow-Release Microcapsules Containing Patchouli Oil [J].
Han, Guangtao ;
Yang, Ziming ;
Peng, Zheng ;
Wang, Guang ;
Zhou, Min ;
Pang, Yuxin ;
Li, Puwang .
BIOTECHNOLOGY, CHEMICAL AND MATERIALS ENGINEERING II, PTS 1 AND 2, 2013, 641-642 :935-+
[8]   Formation of hydrogel particles by thermal treatment of β-lactoglobulin-chitosan complexes [J].
Hong, Youn-Ho ;
McClements, David Julian .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2007, 55 (14) :5653-5660
[9]   Effect of polysaccharide charge on formation and properties of biopolymer nanoparticles created by heat treatment of β-lactoglobulin-pectin complexes [J].
Jones, Owen G. ;
Lesmes, Uri ;
Dubin, Paul ;
McClements, David Julian .
FOOD HYDROCOLLOIDS, 2010, 24 (04) :374-383
[10]   Characterization of gelatin nanofiber prepared from gelatin-formic acid solution [J].
Ki, CS ;
Baek, DH ;
Gang, KD ;
Lee, KH ;
Um, IC ;
Park, YH .
POLYMER, 2005, 46 (14) :5094-5102