Synthesis of 4,4′-Bis[4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-phenylcarbonylamino]-3,3′-dichlorodiphenylmethane and 1,4-Bis{2-[4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-phenylcarbonyloxy]ethoxy}benzene

被引：2

作者：

Kolymshin, O. A. ^{[1
]}

Danilov, V. A. ^{[1
]}

Ignatev, V. A. ^{[1
]}

Kuzmin, M., V ^{[1
]}

机构：

[1] Ulyanov Chuvash State Univ, Moskovskii Pr 15, Cheboksary 428015, Chuvash Republi, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2019年 / 55卷 / 11期

关键词：

p-aminobenzoic acid; maleic acid monoamides; bismaleimide; cyclization; IR and H-1 NMR spectra; BISMALEIMIDES;

D O I：

10.1134/S1070428019110071

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

4,4'-Bis[4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylcarbonylamino]-3,3'-dichlorodiphenylmethane has been obtained by the reaction of 4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzoyl chloride with 4,4'-diamino-3,3'-dichlorodiphenylmethane. 1,4-Bis[2-(4-aminophenylcarbonyloxy)ethoxy]benzene has been prepared by the reaction of potassium 4-aminobenzoate with 1,4-bis(2-chloroethoxy)benzene. The synthesized diamine has been reacted with maleic anhydride to obtain 1,4-bis[4-(2-carboxyethen-1-ylcarbamoyl)phenylcarbonyloxyethoxy]benzene, whose subsequent cyclization with acetic anhydride gave 1,4-bis{2-[4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-phenylcarbonyloxy]ethoxy}benzene.

引用

页码：1686 / 1689

页数：4

共 16 条

[1]

Alwin K., 2010, POLYMER, V51, P1887, DOI [10.1016/j.polymer.2010.03.015, DOI 10.1016/J.POLYMER.2010.03.015]

[2]

Beaicewiez B.C, 1994, Ref. Zh. Khim., Patent No. 5198551

[3]

Holub F.F, 1976, Ref. Zh. Khim., Patent No. 3887582

[4] Facile preparation of poly(N-isopropylacrylamide)-based hydrogels via aqueous Diels-Alder click reaction [J].

Wei, Hong-Liang ;

Yang, Zhe ;

Chu, Hui-Juan ;

Zhu, Jing ;

Li, Zhi-Cheng ;

Cui, Jin-Shi .

POLYMER, 2010, 51 (08) :1694-1702

[5] 4-(3-Dialkylamino-2,5-dioxopyrrolidin-1-yl)benzoic acid esters [J].

Kolyamshin, O. A. ;

Danilov, V. A. ;

Kol'tsov, N. I. .

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 43 (03) :393-396

[6] Synthesis of 1-[2-(2,5-dihydro-2,5-dioxo-1H-pyrrol-1-yl)ethyl]-3,5-bis(prop-2-enyl)hexahydro-1,3,5-triazine-2,4,6-trione [J].

Kolyamshin, O. A. ;

Danilov, V. A. ;

Dmitriev, S. N. ;

Kol'tsov, N. I. .

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2006, 42 (07) :1103-1104

[7] Synthesis of benzene-1,4-diylbis(oxyethane-2,1-diyl) bis[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzoates] [J].

Kolyamshin, O. A. ;

Kuz'min, M. V. ;

Ignat'ev, V. A. ;

Rogozhina, L. G. ;

Kol'tsov, N. I. .

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 51 (06) :901-902

[8]

Kolyamshin O.A., 2012, BUTLEROVSK SOOBSHCH, V32, P26

[9] Esters of 4-(3-dialkylamino-2,5-dioxo-2,3,4,5-tetrahydro-1H-pyrrolyl)phenylacetic acids [J].

Kolyamshin, OA ;

Danilov, VA ;

Dashkova, GY ;

Kol'tsov, NI .

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2005, 41 (11) :1657-1660

[10]

Mikhailin Yu.A., 2006, Heat-Resistant Polymers and Polymer Materials

← 1 2 →