Influence of stoichiometry and molar ratio of barium ferrite thin film synthesized by sol-gel on alumina substrate

被引:0
作者
Ghasemi, A [1 ]
Shams, MR [1 ]
Saatchi, A [1 ]
Salehi, M [1 ]
Hosseinpour, A [1 ]
机构
[1] Isfahan Univ Technol, Dept Mat Engn, Esfahan, Iran
来源
14TH CONGRESS OF INTERNATIONAL FEDERATION FOR HEAT TREATMENT AND SURFACE ENGINEERING, VOLS 1 and 2, PROCEEDINGS | 2004年
关键词
sol-gel; barium ferrite; molar ratio; thin film;
D O I
暂无
中图分类号
TH [机械、仪表工业];
学科分类号
0802 ;
摘要
Amorphous gels were processed with a varying Fe/Ba ratio of 11/5, 28/2, 10.5/1 in water and Solvent. Iron and barium nitrites with specific molar ratio was solved in water and slovent at 60 degrees C for 3 hours untill a dark brown solution was prepared. The sols were introduced to substrate dropwise and spinning with 2000 rpm in 3 min was applied; the work was repeated for 10 times and the samples were dried and sintered. The TGA analysis was used to identify the heating rate of the samples; at temperature of 1150 degrees c for one hour the final phase was attained. the thickness, uniformity, morphology and the composition were examined by SEM and XRD. The study shows that the fabrication barium ferrite film of the molar ratio of Fe/Ba = 10.5/1 is much more suitable than other ratios
引用
收藏
页码:1313 / 1315
页数:3
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