Spatial structure of triglycine determined by the residual dipolar coupling analysis

被引:13
|
作者
Klochkov, VV [1 ]
Khairutdinov, BI [1 ]
Klochkov, AV [1 ]
Shtyrlin, VG [1 ]
Shaykhutdinov, RA [1 ]
机构
[1] Kazan VI Lenin State Univ, Dept Chem, Kazan 420008, Russia
关键词
D O I
10.1007/BF03166971
中图分类号
O64 [物理化学(理论化学)、化学物理学]; O56 [分子物理学、原子物理学];
学科分类号
070203 ; 070304 ; 081704 ; 1406 ;
摘要
The possibility to determine the relatively small organic compound conformations by the approach on the basis of the analysis of the residual dipolar couplings H-1-C-13 in the molecules partially aligned in lyotropic liquid crystalline media has been considered. This approach has been used in the nuclear magnetic resonance investigation of the triglycine structure in lyotropic medium (cetylpyridinium bromide/n-hexanol). The conformation of triglycine in solution has been established as transtrans on the basis of the experimental data of observed couplings.
引用
收藏
页码:113 / 119
页数:7
相关论文
共 50 条
  • [41] The effects of residual dipolar coupling on carnosine in proton muscle spectra
    Lievens, Eline
    Van Vossel, Kim
    van de Casteele, Freek
    Derave, Wim
    Murdoch, James B.
    NMR IN BIOMEDICINE, 2024, 37 (04)
  • [42] Assessment of zinc finger orientations by residual dipolar coupling constants
    Tsui, V
    Zhu, LM
    Huang, TH
    Wright, PE
    Case, DA
    JOURNAL OF BIOMOLECULAR NMR, 2000, 16 (01) : 9 - 21
  • [43] Solution structure of tRNAVal from refinement of homology model against residual dipolar coupling and SAXS data
    Alexander Grishaev
    Jinfa Ying
    Marella D. Canny
    Arthur Pardi
    Ad Bax
    Journal of Biomolecular NMR, 2008, 42
  • [44] Solution structure of tRNAVal from refinement of homology model against residual dipolar coupling and SAXS data
    Grishaev, Alexander
    Ying, Jinfa
    Canny, Marella D.
    Pardi, Arthur
    Bax, Ad
    JOURNAL OF BIOMOLECULAR NMR, 2008, 42 (02) : 99 - 109
  • [45] Validation of helical tilt angles in the solution NMR structure of the Z domain of Staphylococcal protein A by combined analysis of residual dipolar coupling and NOE data
    Zheng, DY
    Aramini, JM
    Montelione, GT
    PROTEIN SCIENCE, 2004, 13 (02) : 549 - 554
  • [46] Residual Dipolar Couplings (RDCs) in Organic Structure Determination
    Thiele, Christina M.
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 2008 (34) : 5673 - 5685
  • [47] Residual Dipolar Couplings in Structure Determination of Natural Products
    Li G.-W.
    Liu H.
    Qiu F.
    Wang X.-J.
    Lei X.-X.
    Natural Products and Bioprospecting, 2018, 8 (4) : 279 - 295
  • [48] Structure and dynamics of carbohydrates using residual dipolar couplings
    Prestegard, James H.
    Yi, Xiaobing
    NMR SPECTROSCOPY AND COMPUTER MODELING OF CARBOHYDRATES: RECENT ADVANCES, 2006, 930 : 40 - 59
  • [49] Residual dipolar couplings in nucleic acid structure determination
    MacDonald, D
    Lu, P
    CURRENT OPINION IN STRUCTURAL BIOLOGY, 2002, 12 (03) : 337 - 343
  • [50] Protein structure prediction using residual dipolar couplings
    Emiris, Loannis Z.
    Pantos, Sotirios I.
    ALGEBRAIC BIOLOGY, PROCEEDINGS, 2007, 4545 : 217 - +